Cyclohexane, 1-methylene-2-[(methylthio)methyl]-

Base Information

Chemical Name:Cyclohexane, 1-methylene-2-[(methylthio)methyl]-
CAS No.:67173-79-9
Molecular Formula:C9H16S
Molecular Weight:156.292
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexane, 1-methylene-2-[(methylthio)methyl]-

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Technology Process of Cyclohexane, 1-methylene-2-[(methylthio)methyl]-

There total 5 articles about Cyclohexane, 1-methylene-2-[(methylthio)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₉S⁽¹⁺⁾*CF₃O₃S^(1-)

: 67173-79-9
methyl(2-methylenecyclohexyl)methyl sulfide

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; dichloromethane; tert-butyl alcohol; at -40 - 20 ℃; for 10h; Schlenk technique;
DOI:10.1021/ol5031348

Reference yield:

: 1192-37-6
methylenecyclohexane

: 67173-79-9
methyl(2-methylenecyclohexyl)methyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 2-chloropyridine / dichloromethane / 5 h / -80 - 20 °C / Schlenk technique

2: potassium tert-butylate / tetrahydrofuran; dichloromethane; tert-butyl alcohol / 10 h / -40 - 20 °C / Schlenk technique

With 2-chloropyridine; potassium tert-butylate; In tetrahydrofuran; dichloromethane; tert-butyl alcohol;
DOI:10.1021/ol5031348

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 67173-79-9
methyl(2-methylenecyclohexyl)methyl sulfide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere; Cooling with ice

1.2: 0.5 h / 20 °C / Inert atmosphere

2.1: 2-chloropyridine / dichloromethane / 5 h / -80 - 20 °C / Schlenk technique

3.1: potassium tert-butylate / tetrahydrofuran; dichloromethane; tert-butyl alcohol / 10 h / -40 - 20 °C / Schlenk technique

With 2-chloropyridine; potassium tert-butylate; sodium hydride; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1021/ol5031348