anguibactin

Base Information

Chemical Name:anguibactin
CAS No.:104245-09-2
Molecular Formula:C15H16N4O4S
Molecular Weight:348.382
Hs Code.:

Synonyms:anguibactin

Suppliers and Price of anguibactin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
ANGUIBACTIN 95.00%
5MG
$ 496.69

Total 3 raw suppliers

Chemical Property of anguibactin

Chemical Property:

Vapor Pressure:1.07E-24mmHg at 25°C
Boiling Point:766.4°Cat760mmHg
Flash Point:417.3°C
PSA：143.85000
Density:1.609g/cm³
LogP:0.99620

Purity/Quality:

95% ^*data from raw suppliers

ANGUIBACTIN 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of anguibactin

There total 5 articles about anguibactin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₂₃H₂₄N₄O₄S

: 104245-09-2
anguibactin

Guidance literature:: With boron trichloride; tetra-(n-butyl)ammonium iodide; In dichloromethane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b02789

Reference yield:

: 1268613-18-8
C₁₂H₁₅N₃O

: 104245-09-2
anguibactin

Guidance literature:: Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 4 h / 20 °C / Inert atmosphere

2: tetra-(n-butyl)ammonium iodide; boron trichloride / dichloromethane / 2 h / -78 °C / Inert atmosphere

With boron trichloride; tetra-(n-butyl)ammonium iodide; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane;
DOI:10.1021/acs.orglett.8b02789

Reference yield:

: 6812-16-4
2-Hydroxy-3-methoxybenzonitrile

: 104245-09-2
anguibactin

Guidance literature:: Multi-step reaction with 3 steps

1: aq. phosphate buffer; methanol / 24 h / 50 °C / pH 6.4 / Inert atmosphere

2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 4 h / 20 °C / Inert atmosphere

3: tetra-(n-butyl)ammonium iodide; boron trichloride / dichloromethane / 2 h / -78 °C / Inert atmosphere

With boron trichloride; tetra-(n-butyl)ammonium iodide; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; aq. phosphate buffer; dichloromethane;
DOI:10.1021/acs.orglett.8b02789