Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-7-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-4,7 -dihydro-2-[[[(2S)-2-hydroxy-2-phenylethyl]methylamino]methyl]-4-oxo-

Base Information

• Chemical Name: Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-7-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-4,7 -dihydro-2-[[[(2S)-2-hydroxy-2-phenylethyl]methylamino]methyl]-4-oxo-
• CAS No.: 672326-26-0
• Molecular Formula: C31H34ClN3O5S
• Molecular Weight: 596.147

Synonyms:

Chemical Property of Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-7-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-4,7 -dihydro-2-[[[(2S)-2-hydroxy-2-phenylethyl]methylamino]methyl]-4-oxo-

Chemical Property:

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Technology Process of Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-7-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-4,7 -dihydro-2-[[[(2S)-2-hydroxy-2-phenylethyl]methylamino]methyl]-4-oxo-

There total 1 articles about Thieno[2,3-b]pyridine-5-carboxamide, N-[(4-chlorophenyl)methyl]-7-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-4,7 -dihydro-2-[[[(2S)-2-hydroxy-2-phenylethyl]methylamino]methyl]-4-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(chloromethyl)-N-((4-chlorophenyl)methyl)-7-((2,2-dimethyl-1,3-dioxolan-4-yl)methyl)-4,7-dihydro-4-oxothieno[2,3-b]-pyridine-5-carboxamide (672326-05-5) + N-methyl (S)-2-hydroxy-2-phenylethylamine (65058-52-8,6589-55-5) → N-(4-chlorobenzyl)-7-((2,2-dimethyl-1,3-dioxolan-4-yl)methyl)-2-((((2S)-2-hydroxy-2-phenylethyl)(methyl)amino)methyl)-4-oxo-4,7-dihydrothieno[2,3-b]pyridine-5-carboxamide (672326-26-0)

Guidance literature:

With caesium carbonate; In DMF (N,N-dimethyl-formamide); at 60 ℃; for 17h; 3 A sieves;

Reference yield:

N-(4-chlorobenzyl)-7-((2,2-dimethyl-1,3-dioxolan-4-yl)methyl)-2-((((2S)-2-hydroxy-2-phenylethyl)(methyl)amino)methyl)-4-oxo-4,7-dihydrothieno[2,3-b]pyridine-5-carboxamide (672326-26-0) → N-(4-chlorobenzyl)-7-(2,3-dihydroxypropyl)-2-((((2S)-2-hydroxy-2-phenylethyl)(methyl)amino)methyl)-4-oxo-4,7-dihydrothieno[2,3-b]pyridine-5-carboxamide

Guidance literature:

With perchloric acid; In tetrahydrofuran; water; at 20 ℃; for 6h;

upstream raw materials:

2-(chloromethyl)-N-((4-chlorophenyl)methyl)-7-((2,2-dimethyl-1,3-dioxolan-4-yl)methyl)-4,7-dihydro-4-oxothieno[2,3-b]-pyridine-5-carboxamide

N-methyl (S)-2-hydroxy-2-phenylethylamine

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