N-[(m-Nitrophenyl)sulfonyl]carbamic acid ethyl ester

Base Information

• Chemical Name: N-[(m-Nitrophenyl)sulfonyl]carbamic acid ethyl ester
• CAS No.: 22819-24-5
• Molecular Formula: C9H10 N2 O6 S
• Molecular Weight: 274.254
• Hs Code.: 2935009090
• Mol file: 22819-24-5.mol

Synonyms:Carbamicacid, [(m-nitrophenyl)sulfonyl]-, ethyl ester (6CI,7CI,8CI)

Chemical Property of N-[(m-Nitrophenyl)sulfonyl]carbamic acid ethyl ester

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 130.16000
• Density: 1.455g/cm³
• LogP: 2.83800

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-[(m-Nitrophenyl)sulfonyl]carbamic acid ethyl ester

There total 3 articles about N-[(m-Nitrophenyl)sulfonyl]carbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Nitro-benzolsulfinsaeure-chlorid (100191-54-6) → (3-nitro-benzenesulfonyl)-carbamic acid ethyl ester (22819-24-5)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene

2: aq. KOH

With potassium hydroxide; In benzene;

Reference yield:

3-Nitro-benzolsulfonsaeure-chlorid-aethoxycarbonylimid (93905-67-0) → (3-nitro-benzenesulfonyl)-carbamic acid ethyl ester (22819-24-5)

Guidance literature:

With potassium hydroxide;

Reference yield:

→ (3-nitro-benzenesulfonyl)-carbamic acid ethyl ester (22819-24-5)

Guidance literature:

S-Methylthiocarbamat (3, R=m-NO2), Ethanol;

upstream raw materials:

3-Nitro-benzolsulfonsaeure-chlorid-aethoxycarbonylimid

3-Nitro-benzolsulfinsaeure-chlorid

Downstream raw materials:

(1S,2S,3R,4R,5R)-3-(2-chloro-5-fluoropyrimidin-4-ylamino)-5-(3-(3-nitrophenylsulfonyl)ureido)bicyclo[2.2.1]heptane-2-carboxamide

(3-amino-benzenesulfonyl)-carbamic acid ethyl ester

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