1-(4-Methoxy-2-nitrophenyl)ethanone

Base Information

Chemical Name:1-(4-Methoxy-2-nitrophenyl)ethanone
CAS No.:67323-06-2
Molecular Formula:C9H9NO4
Molecular Weight:195.175
Hs Code.:
DSSTox Substance ID:DTXSID50505479
Wikidata:Q82360651
Mol file:67323-06-2.mol

Synonyms:1-(4-methoxy-2-nitrophenyl)ethanone;67323-06-2;4'-METHOXY-2'-NITROACETOPHENONE;1-(4-methoxy-2-nitrophenyl)ethan-1-one;SCHEMBL1632528;DTXSID50505479;IOPKQYZGKNCNAB-UHFFFAOYSA-N;AKOS006294674;FT-0641115;A835711

Suppliers and Price of 1-(4-Methoxy-2-nitrophenyl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4'-METHOXY-2'-NITROACETOPHENONE 98.00%
10G
$ 2556.02

Alichem
1-(4-Methoxy-2-nitrophenyl)ethanone
1g
$ 400.00

AHH
4'-Methoxy-2'-nitroacetophenone 98%
10g
$ 998.00

Total 7 raw suppliers

Chemical Property of 1-(4-Methoxy-2-nitrophenyl)ethanone

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:49-50 °C(Solv: ethyl ether (60-29-7); ligroine (8032-32-4))
Boiling Point:352.133oC at 760 mmHg
Flash Point:173.057oC
PSA：72.12000
Density:1.245g/cm3
LogP:2.32920
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:195.05315777
Heavy Atom Count:14
Complexity:236

Purity/Quality:

98%min ^*data from raw suppliers

4'-METHOXY-2'-NITROACETOPHENONE 98.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=C(C=C(C=C1)OC)[N+](=O)[O-]

Technology Process of 1-(4-Methoxy-2-nitrophenyl)ethanone

There total 5 articles about 1-(4-Methoxy-2-nitrophenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1439930-70-7
(E)-1-(4-methoxy-2-nitrophenyl)ethanone O-methyl oxime

: 67323-06-2
1-(4-methoxy-2-nitrophenyl)ethanone

Guidance literature:: With hydrogenchloride; water; In dichloromethane; at 100 ℃; for 24h; Sealed tube;
DOI:10.1021/jo400594j

Reference yield:

: 80965-21-5
(E)-1-(4-methoxyphenyl)ethan-1-one O-methyl oxime

: 67323-06-2
1-(4-methoxy-2-nitrophenyl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: silver(I) nitrite; dipotassium peroxodisulfate; palladium(II) trifluoroacetate / 1,2-dichloro-ethane / 48 h / 110 °C / Schlenk technique; Sealed tube

2: hydrogenchloride; water / dichloromethane / 24 h / 100 °C / Sealed tube

With hydrogenchloride; dipotassium peroxodisulfate; silver(I) nitrite; palladium(II) trifluoroacetate; water; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo400594j