1,1,2-Ethanetricarboxylic acid, 1-[[1-oxo-3-(phenylmethoxy)-2-[[(phenylmethoxy)carbonyl]amino]propyl] amino]-, 1,1-bis(phenylmethyl) ester, (S)-

Base Information

Chemical Name:1,1,2-Ethanetricarboxylic acid, 1-[[1-oxo-3-(phenylmethoxy)-2-[[(phenylmethoxy)carbonyl]amino]propyl] amino]-, 1,1-bis(phenylmethyl) ester, (S)-
CAS No.:67354-59-0
Molecular Formula:C₃₇H₃₆N₂O₁₀
Molecular Weight:668.7
Hs Code.:

1,1,2-Ethanetricarboxylic acid,
1-[[1-oxo-3-(phenylmethoxy)-2-[[(phenylmethoxy)carbonyl]amino]propyl]
amino]-, 1,1-bis(phenylmethyl) ester, (S)-

Synonyms:

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Chemical Property of 1,1,2-Ethanetricarboxylic acid, 1-[[1-oxo-3-(phenylmethoxy)-2-[[(phenylmethoxy)carbonyl]amino]propyl] amino]-, 1,1-bis(phenylmethyl) ester, (S)-

Chemical Property:

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Technology Process of 1,1,2-Ethanetricarboxylic acid, 1-[[1-oxo-3-(phenylmethoxy)-2-[[(phenylmethoxy)carbonyl]amino]propyl] amino]-, 1,1-bis(phenylmethyl) ester, (S)-

There total 4 articles about 1,1,2-Ethanetricarboxylic acid, 1-[[1-oxo-3-(phenylmethoxy)-2-[[(phenylmethoxy)carbonyl]amino]propyl] amino]-, 1,1-bis(phenylmethyl) ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67354-58-9
N-(O³-Benzyl-N-benzyloxycarbonylseryl)-2-benzyloxycarbonylasparaginsaeure-O¹-benzyl-O⁴-tert-butylester

: 67354-59-0
N-(O³-Benzyl-N-benzyloxycarbonylseryl)-2-benzyloxycarbonylasparaginsaeure-O¹-monobenzylester

Guidance literature:: With toluene-4-sulfonic acid; In acetic acid;
DOI:10.1016/S0040-4020(01)93609-9

Reference yield:

: 67354-46-5
N-(2,2,2-Trichlorethoxycarbonyl)-aminomalonsaeuredibenzylester

: 67354-59-0
N-(O³-Benzyl-N-benzyloxycarbonylseryl)-2-benzyloxycarbonylasparaginsaeure-O¹-monobenzylester

Guidance literature:: Multi-step reaction with 3 steps

1: (i) NaH, DMF, (ii) /BRN= 1753006/

2: (i) Zn, aq. AcOH, (ii) /BRN= 2302653/, DCC, THF

3: TsOH / acetic acid

With toluene-4-sulfonic acid; In acetic acid;
DOI:10.1016/S0040-4020(01)93609-9

Reference yield:

: 67354-47-6
2-Benzyloxycarbonyl-N-(2,2,2-trichlorethoxycarbonyl)-asparaginsaeure-O¹-benzyl-O⁴-tert-butylester

: 67354-59-0
N-(O³-Benzyl-N-benzyloxycarbonylseryl)-2-benzyloxycarbonylasparaginsaeure-O¹-monobenzylester

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Zn, aq. AcOH, (ii) /BRN= 2302653/, DCC, THF

2: TsOH / acetic acid

With toluene-4-sulfonic acid; In acetic acid;
DOI:10.1016/S0040-4020(01)93609-9