1-[3-[(3-Aminopropyl)amino]propyl]hexahydro-1H-azepin-2-one

Base Information

• Chemical Name: 1-[3-[(3-Aminopropyl)amino]propyl]hexahydro-1H-azepin-2-one
• CAS No.: 67370-65-4
• Molecular Formula: C12H25N3O
• Molecular Weight: 227.34600

Synonyms:1-[3-(3-Amino-propylamino)-propyl]-azepan-2-one;N-<3-(3-Amino-propylamino)-propyl>-ε-caprolactam;

Chemical Property of 1-[3-[(3-Aminopropyl)amino]propyl]hexahydro-1H-azepin-2-one

Chemical Property:

• Boiling Point: 125 °C (0.001 mmHg)
• PSA: 58.36000
• LogP: 1.74660

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[3-[(3-Aminopropyl)amino]propyl]hexahydro-1H-azepin-2-one

There total 1 articles about 1-[3-[(3-Aminopropyl)amino]propyl]hexahydro-1H-azepin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-[3-(3-amino-propylamino)-propyl]-azepan-2-one (67370-65-4)

Guidance literature:

N-<3-(2-Cyan-ethylamino)-propyl>-ε-caprolactam, H2SO4 in A., H2 - Pt;

DOI:10.1002/hlca.19780610315

Reference yield:

1-[3-(3-amino-propylamino)-propyl]-azepan-2-one (67370-65-4) + acetic anhydride (108-24-7) + Trimethylenediamine (109-76-2,54018-94-9) → 6-(Acetyl-{3-[acetyl-(3-acetylamino-propyl)-amino]-propyl}-amino)-hexanoic acid (3-acetylamino-propyl)-amide (67370-66-5)

Guidance literature:

Multistep reaction; (i) KH, (ii) /BRN= 385737/, Py;

DOI:10.1002/hlca.19780610315

Downstream raw materials:

6-(Acetyl-{3-[acetyl-(3-acetylamino-propyl)-amino]-propyl}-amino)-hexanoic acid (3-acetylamino-propyl)-amide

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