Limazocic

Base Information

Chemical Name:Limazocic
CAS No.:128620-82-6
Molecular Formula:C8H13 N O3 S2
Molecular Weight:235.328
Hs Code.:

Synonyms:1,2,5-Dithiazocine-4-carboxylicacid, hexahydro-7,7-dimethyl-6-oxo-, (R)-; (-)-(R)-Hexahydro-7,7-dimethyl-6-oxo-1,2,5-dithiazocine-4-carboxylicacid; (4R)-Hexahydro-7,7-dimethyl-6-oxo-1,2,5-dithiazocine-4-carboxylic acid;Limazocic; SA 3443

Suppliers and Price of Limazocic

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Limazocic

Chemical Property:

Vapor Pressure:6.03E-11mmHg at 25°C
Boiling Point:490.1°Cat760mmHg
Flash Point:250.2°C
Density:1.278g/cm³

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Limazocic

There total 3 articles about Limazocic which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.2%

: 124775-63-9
N-(3-mercapto-2,2-dimethylpropionyl)-L-cysteine

: 128620-82-6
SA₃₄₄₃

Guidance literature:: With iodine; triethylamine; In ethyl acetate; at -10 - 5 ℃; for 1h;
DOI:10.1248/cpb.41.1066

Reference yield:

: 13511-38-1
3-chloropivalic acid

: 128620-82-6
SA₃₄₄₃

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) thiourea, 2.) aq. NaOH / 1.) 180-200 deg C, 2.5 h, 2.) H₂O, reflux, 2.5 h

2: 1.) N,N'-dicyclohexylcarbodiimide, 2.) K₂CO₃ / 1.) AcOEt, RT, 40 min, 2.) water, DMF, RT, overnight

3: 63.2 percent / I₂, Et₃N / ethyl acetate / 1 h / -10 - 5 °C

With sodium hydroxide; iodine; potassium carbonate; triethylamine; thiourea; dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1248/cpb.41.1066

Reference yield:

: 35040-68-7
2,2-dimethyl-3-mercaptopropanoic acid

: 128620-82-6
SA₃₄₄₃

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N,N'-dicyclohexylcarbodiimide, 2.) K₂CO₃ / 1.) AcOEt, RT, 40 min, 2.) water, DMF, RT, overnight

2: 63.2 percent / I₂, Et₃N / ethyl acetate / 1 h / -10 - 5 °C

With iodine; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1248/cpb.41.1066