Piperazinone, 3,5-diethyl-1-(phenylmethyl)-, (3R,5R)-

Base Information

Chemical Name:Piperazinone, 3,5-diethyl-1-(phenylmethyl)-, (3R,5R)-
CAS No.:674792-16-6
Molecular Formula:C15H22N2O
Molecular Weight:246.352
Hs Code.:

Synonyms:

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Chemical Property of Piperazinone, 3,5-diethyl-1-(phenylmethyl)-, (3R,5R)-

Chemical Property:

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Technology Process of Piperazinone, 3,5-diethyl-1-(phenylmethyl)-, (3R,5R)-

There total 7 articles about Piperazinone, 3,5-diethyl-1-(phenylmethyl)-, (3R,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 674792-15-5
C₂₆H₃₈N₂O₂

: 674792-16-6
C₁₅H₂₂N₂O

Guidance literature:: C₂₆H₃₈N₂O₂; With hydrogenchloride; hydrogen; palladium(II) hydroxide/carbon; In 1,4-dioxane; ethanol; for 18h;

In acetic acid; toluene; for 48h; Heating / reflux;

Reference yield:

: 674792-14-4
C₁₈H₂₄N₂

: 674792-16-6
C₁₅H₂₂N₂O

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 5 h / 0 - 20 °C

2: hydrogenchloride; palladium on carbon; hydrogen / water

3: toluene-4-sulfonic acid / Reflux

With hydrogenchloride; palladium on carbon; hydrogen; toluene-4-sulfonic acid; triethylamine; In dichloromethane; water;
DOI:10.1016/j.bmcl.2011.02.090

Reference yield:

: 674792-12-2
C₂₃H₃₀N₂O₃

: 674792-16-6
C₁₅H₂₂N₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / dichloromethane

2.1: borane-THF

2.3: Reflux

3.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C

4.1: hydrogenchloride; palladium on carbon; hydrogen / water

5.1: toluene-4-sulfonic acid / Reflux

With hydrogenchloride; borane-THF; palladium on carbon; hydrogen; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; In dichloromethane; water;
DOI:10.1016/j.bmcl.2011.02.090