α-Cannabispiranol

Base Information

Chemical Name:α-Cannabispiranol
CAS No.:69636-83-5
Molecular Formula:C₁₅H₂₀O₃
Molecular Weight:248.322
Hs Code.:
Mol file:69636-83-5.mol

Synonyms:a-Cannabispiranol

Suppliers and Price of α-Cannabispiranol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
alpha-Cannabispiranol ≥98%
5mg
$ 463.00

Total 11 raw suppliers

Chemical Property of α-Cannabispiranol

Chemical Property:

PSA：49.69000
LogP:2.51970

Purity/Quality:

≥98% ^*data from raw suppliers

alpha-Cannabispiranol ≥98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of α-Cannabispiranol

There total 20 articles about α-Cannabispiranol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

: 61262-81-5
cannabispirone

: 69636-83-5
α-cannabispiranol

: 64052-90-0
β-cannabispiranol

Guidance literature:: With sodium tetrahydroborate; In methanol; for 3h;

Reference yield:

: 880-87-5
5,7-dimethoxyindan-1-one

: 69636-83-5
α-cannabispiranol

Guidance literature:: Multi-step reaction with 8 steps

1: 84 percent / potassium t-butoxide / 2-methyl-propan-2-ol; 1,2-dimethoxy-ethane / 50 h / 20 °C

2: 84 percent / n-butyl-lithium, diethylamine / hexane; tetrahydrofuran; hexamethylphosphoric acid triamide

3: 1.) di-isobutylaluminium hydride, 2.) aqueous acetic acid / 1.) toluene, -78 deg C, 2.5 h, 2.) room temperature, 30 min

4: 98 percent / m-hydrochloric acid / tetrahydrofuran / 12 h

5: 92 percent / aqueous potassium hydroxide / methanol / 24 h / 20 °C

6: 85 percent / lithium 1,1-dimethylethanethiolate / hexamethylphosphoric acid triamide / 2 h / 70 °C

7: 51 mg / H₂ / 5percent Pd-C / ethyl acetate

8: 33 percent / sodium borohydride / methanol / 3 h

With hydrogenchloride; lithium tert-butylsulfide; potassium hydroxide; sodium tetrahydroborate; n-butyllithium; diisobutylaluminum hydride; potassium tert-butylate; hydrogen; acetic acid; diethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; hexane; ethyl acetate; tert-butyl alcohol;

Reference yield:

: 717-94-2
3-(3,5-dimethoxyphenyl)propionic acid

: 69636-83-5
α-cannabispiranol

Guidance literature:: Multi-step reaction with 9 steps

1: 91 percent / polyphosphoric acid / 2 h / 70 °C

2: 84 percent / potassium t-butoxide / 2-methyl-propan-2-ol; 1,2-dimethoxy-ethane / 50 h / 20 °C

3: 84 percent / n-butyl-lithium, diethylamine / hexane; tetrahydrofuran; hexamethylphosphoric acid triamide

4: 1.) di-isobutylaluminium hydride, 2.) aqueous acetic acid / 1.) toluene, -78 deg C, 2.5 h, 2.) room temperature, 30 min

5: 98 percent / m-hydrochloric acid / tetrahydrofuran / 12 h

6: 92 percent / aqueous potassium hydroxide / methanol / 24 h / 20 °C

7: 85 percent / lithium 1,1-dimethylethanethiolate / hexamethylphosphoric acid triamide / 2 h / 70 °C

8: 51 mg / H₂ / 5percent Pd-C / ethyl acetate

9: 33 percent / sodium borohydride / methanol / 3 h

With hydrogenchloride; lithium tert-butylsulfide; potassium hydroxide; sodium tetrahydroborate; n-butyllithium; PPA; diisobutylaluminum hydride; potassium tert-butylate; hydrogen; acetic acid; diethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; hexane; ethyl acetate; tert-butyl alcohol;