(2S)-{[(2S)-2-amino-3-(1H-indol-3-yl)propanoyl]amino}[(3S,4R,5R)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-3,4-dihydroxytetrahydrofuran-2-yl]ethanoic acid (non-preferred name)

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Chemical Name:(2S)-{[(2S)-2-amino-3-(1H-indol-3-yl)propanoyl]amino}[(3S,4R,5R)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-3,4-dihydroxytetrahydrofuran-2-yl]ethanoic acid (non-preferred name)
CAS No.:86632-67-9
Molecular Formula:4C₂HF₃O₂*5C₂₁H₂₃N₅O₈
Molecular Weight:2823.31
Hs Code.:

(2S)-{[(2S)-2-amino-3-(1H-indol-3-yl)propanoyl]amino}[(3S,4R,5R)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-3,4-dihydroxytetrahydrofuran-2-yl]ethanoic acid (non-preferred name)

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Chemical Property of (2S)-{[(2S)-2-amino-3-(1H-indol-3-yl)propanoyl]amino}[(3S,4R,5R)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-3,4-dihydroxytetrahydrofuran-2-yl]ethanoic acid (non-preferred name)

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.631g/cm³

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MSDS Files:: SDS file from LookChem

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Technology Process of (2S)-{[(2S)-2-amino-3-(1H-indol-3-yl)propanoyl]amino}[(3S,4R,5R)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-3,4-dihydroxytetrahydrofuran-2-yl]ethanoic acid (non-preferred name)

There total 2 articles about (2S)-{[(2S)-2-amino-3-(1H-indol-3-yl)propanoyl]amino}[(3S,4R,5R)-5-(2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-3,4-dihydroxytetrahydrofuran-2-yl]ethanoic acid (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-Benzyloxycarbonylamino-3-(3H-indol-3-yl)-propionic acid 4-nitro-phenyl ester

: 86632-67-9
(S)-[(S)-2-Amino-3-(1H-indol-3-yl)-propionylamino]-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-acetic acid; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / dimethylformamide; H₂O / 24 h / Ambient temperature

2: H₂ / Pd black / methanol / 0.5 h / Ambient temperature

With 4-methyl-morpholine; hydrogen; palladium; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00364a030