Decanoic acid, 8-oxo-2-[[(phenylmethoxy)carbonyl]amino]-, (2S)-

Base Information

Chemical Name:Decanoic acid, 8-oxo-2-[[(phenylmethoxy)carbonyl]amino]-, (2S)-
CAS No.:676268-52-3
Molecular Formula:C18H25NO5
Molecular Weight:335.4
Hs Code.:

Synonyms:

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Chemical Property of Decanoic acid, 8-oxo-2-[[(phenylmethoxy)carbonyl]amino]-, (2S)-

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Technology Process of Decanoic acid, 8-oxo-2-[[(phenylmethoxy)carbonyl]amino]-, (2S)-

There total 15 articles about Decanoic acid, 8-oxo-2-[[(phenylmethoxy)carbonyl]amino]-, (2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: ethyl (S)-2-(((benzyloxy)carbonyl)amino)-8-oxodecanoate

: 676268-52-3
(S)-2-(((benzyloxy)carbonyl)amino)-8-oxodecanoic acid

Guidance literature:: With lithium hydroxide monohydrate; In tetrahydrofuran; water; at 0 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jacs.1c03903

Reference yield: 39.0%

: (S)-(+)-N-benzyloxycarbonyl-9-ethyl-3-deca-1,9-dienylamine

: 676268-52-3
(S)-2-(((benzyloxy)carbonyl)amino)-8-oxodecanoic acid

Guidance literature:: With ruthenium trichloride; periodic acid; In tetrachloromethane; acetonitrile; at 20 ℃; for 3h;
DOI:10.1039/b310624a

Reference yield:

: 1940-18-7
1-ethylcyclohexanol

: 676268-52-3
(S)-2-(((benzyloxy)carbonyl)amino)-8-oxodecanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: [bis(acetoxy)iodo]benzene; iodine / dichloromethane / 2 h / 20 °C / Irradiation; Inert atmosphere

2: iodine / tetrahydrofuran / 12 h / 50 °C / Inert atmosphere; Sealed tube

3: 2,6-bis((4R,5S)-4-isopropyl-5-phenyl-4,5-dihydrooxazol-2-yl)pyridine; nickel(II) bromide dimethoxyethane / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere; Sealed tube

4: lithium hydroxide monohydrate / tetrahydrofuran; water / 5 h / 0 °C / Inert atmosphere

With nickel(II) bromide dimethoxyethane; lithium hydroxide monohydrate; [bis(acetoxy)iodo]benzene; iodine; 2,6-bis((4R,5S)-4-isopropyl-5-phenyl-4,5-dihydrooxazol-2-yl)pyridine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jacs.1c03903