3-TERT-BUTOXYCARBONYLAMINO-HEPTANOIC ACID

Base Information

Chemical Name:3-TERT-BUTOXYCARBONYLAMINO-HEPTANOIC ACID
CAS No.:676348-90-6
Molecular Formula:C12H23NO4
Molecular Weight:245.31500
Hs Code.:2924190090
Mol file:676348-90-6.mol

Synonyms:3-tert-Butoxycarbonylamino-heptanoic acid;N-tert-butoxycarbonyl 3-amino-heptanoic acid;AA140;

Suppliers and Price of 3-TERT-BUTOXYCARBONYLAMINO-HEPTANOIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
3-tert-Butoxycarbonylaminoheptanoic acid
1 g
$ 616.00

Apolloscientific
3-tert-Butoxycarbonylamino-heptanoicacid
1g
$ 559.00

American Custom Chemicals Corporation
3-TERT-BUTOXYCARBONYLAMINO-HEPTANOIC ACID 95.00%
5MG
$ 495.59

Total 4 raw suppliers

Chemical Property of 3-TERT-BUTOXYCARBONYLAMINO-HEPTANOIC ACID

Chemical Property:

Vapor Pressure:7.9E-07mmHg at 25°C
Boiling Point:380.1oC at 760 mmHg
PKA:4.45±0.10(Predicted)
Flash Point:183.7oC
PSA：75.63000
Density:1.048g/cm3
LogP:2.93550

Purity/Quality:

98%Min ^*data from raw suppliers

3-tert-Butoxycarbonylaminoheptanoic acid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-TERT-BUTOXYCARBONYLAMINO-HEPTANOIC ACID

There total 4 articles about 3-TERT-BUTOXYCARBONYLAMINO-HEPTANOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [1-(2-oxo-ethyl)-pentyl]-carbamic acid tert-butyl ester

: 676348-90-6
N-tert-butoxycarbonyl 3-amino-heptanoic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tert-butyl alcohol; at 20 ℃; for 1h;
DOI:10.1002/chem.200401295

Reference yield:

: (1-butyl-but-3-enyl)-carbamic acid tert-butyl ester

: 676348-90-6
N-tert-butoxycarbonyl 3-amino-heptanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: O₃ / CH₂Cl₂; methanol / 2 h / -78 °C

1.2: Me₂S / CH₂Cl₂; methanol / 1 h / -78 - 20 °C

2.1: aq. NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol / 1 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; ozone; In methanol; dichloromethane; tert-butyl alcohol;
DOI:10.1002/chem.200401295

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 676348-90-6
N-tert-butoxycarbonyl 3-amino-heptanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethyl ether / 6 h / 20 °C

2.1: O₃ / CH₂Cl₂; methanol / 2 h / -78 °C

2.2: Me₂S / CH₂Cl₂; methanol / 1 h / -78 - 20 °C

3.1: aq. NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol / 1 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; ozone; In methanol; diethyl ether; dichloromethane; tert-butyl alcohol;
DOI:10.1002/chem.200401295