hydroxy(1H-indol-3-yl)acetic acid

Base Information

• Chemical Name: hydroxy(1H-indol-3-yl)acetic acid
• CAS No.: 27004-49-5
• Molecular Formula: C₁₀H₈NO₃*Na
• Molecular Weight: 213.168

Synonyms:1H-Indole-3-aceticacid, a-hydroxy-, monosodium salt (9CI);Indole-3-glycolic acid, monosodium salt (8CI); NSC 87621

Chemical Property of hydroxy(1H-indol-3-yl)acetic acid

Chemical Property:

• Vapor Pressure: 5.76E-10mmHg at 25°C
• Boiling Point: 478.5°Cat760mmHg
• Flash Point: 243.2°C
• Density: 1.498g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of hydroxy(1H-indol-3-yl)acetic acid

There total 3 articles about hydroxy(1H-indol-3-yl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

hydroxy-(1H-indol-3-yl)-acetic acid ethyl ester → sodium 2-hydroxy-2-(1H-indol-3-yl)acetate (27004-49-5)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water; at 25 ℃; for 12h; Inert atmosphere;

DOI:10.1002/chem.201706149

Reference yield:

→ sodium 2-hydroxy-2-(1H-indol-3-yl)acetate (27004-49-5)

Guidance literature:

With water; palladium; Hydration;

DOI:10.1021/jo01102a025

Reference yield:

indole (120-72-9) → sodium 2-hydroxy-2-(1H-indol-3-yl)acetate (27004-49-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. phosphate buffer; toluene / 4 h / 25 °C / pH 7.4 / Inert atmosphere

2: sodium hydroxide / water; tetrahydrofuran / 12 h / 25 °C / Inert atmosphere

With sodium hydroxide; In tetrahydrofuran; aq. phosphate buffer; water; toluene;

DOI:10.1002/chem.201706149

upstream raw materials:

indole

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