2,5,8,11-Tetraazatridecan-13-oic acid, 11-[[2-amino-6-(phenylmethoxy)-9H-purin-9-yl]acetyl]-1-(4-methoxyphen yl)-7-oxo-1,1-diphenyl-5-[[6-[[(phenylmethoxy)carbonyl]amino]-9H-purin- 9-yl]acetyl]-, methyl ester

Base Information

Chemical Name:2,5,8,11-Tetraazatridecan-13-oic acid, 11-[[2-amino-6-(phenylmethoxy)-9H-purin-9-yl]acetyl]-1-(4-methoxyphen yl)-7-oxo-1,1-diphenyl-5-[[6-[[(phenylmethoxy)carbonyl]amino]-9H-purin- 9-yl]acetyl]-, methyl ester
CAS No.:676555-67-2
Molecular Formula:C58H58N14O9
Molecular Weight:1095.19
Hs Code.:

2,5,8,11-Tetraazatridecan-13-oic acid,
11-[[2-amino-6-(phenylmethoxy)-9H-purin-9-yl]acetyl]-1-(4-methoxyphen
yl)-7-oxo-1,1-diphenyl-5-[[6-[[(phenylmethoxy)carbonyl]amino]-9H-purin-
9-yl]acetyl]-, methyl ester

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Chemical Property of 2,5,8,11-Tetraazatridecan-13-oic acid, 11-[[2-amino-6-(phenylmethoxy)-9H-purin-9-yl]acetyl]-1-(4-methoxyphen yl)-7-oxo-1,1-diphenyl-5-[[6-[[(phenylmethoxy)carbonyl]amino]-9H-purin- 9-yl]acetyl]-, methyl ester

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Technology Process of 2,5,8,11-Tetraazatridecan-13-oic acid, 11-[[2-amino-6-(phenylmethoxy)-9H-purin-9-yl]acetyl]-1-(4-methoxyphen yl)-7-oxo-1,1-diphenyl-5-[[6-[[(phenylmethoxy)carbonyl]amino]-9H-purin- 9-yl]acetyl]-, methyl ester

There total 4 articles about 2,5,8,11-Tetraazatridecan-13-oic acid, 11-[[2-amino-6-(phenylmethoxy)-9H-purin-9-yl]acetyl]-1-(4-methoxyphen yl)-7-oxo-1,1-diphenyl-5-[[6-[[(phenylmethoxy)carbonyl]amino]-9H-purin- 9-yl]acetyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: [[2-(2-Amino-6-benzyloxy-purin-9-yl)-acetyl]-(2-amino-ethyl)-amino]-acetic acid methyl ester; compound with trifluoro-acetic acid

: 676555-52-5
[[2-(6-Benzyloxycarbonylamino-purin-9-yl)-acetyl]-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid

: 676555-67-2
[[2-(2-Amino-6-benzyloxy-purin-9-yl)-acetyl]-(2-{2-[[2-(6-benzyloxycarbonylamino-purin-9-yl)-acetyl]-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid methyl ester

Guidance literature:: With bromo-tris-dimethylamino-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at -15 ℃; for 0.166667h;
DOI:10.1039/b311775h

Reference yield:

: 149376-67-0
[6-N-(benzyloxycarbonyl)-adenin-9-yl]-acetic acid

: 676555-67-2
[[2-(2-Amino-6-benzyloxy-purin-9-yl)-acetyl]-(2-{2-[[2-(6-benzyloxycarbonylamino-purin-9-yl)-acetyl]-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / diisopropylethylamine; bromo-tris-(dimethylamino)-phosphonium-hexafluorophosphate / dimethylformamide / 2 h / 20 °C

2: aq. LiOH / dioxane / 2 h / 20 °C

3: 91 percent / diisopropylethylamine; bromo-tris-(dimethylamino)-phosphonium-hexafluorophosphate / dimethylformamide / 0.17 h / -15 °C

With lithium hydroxide; bromo-tris-dimethylamino-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/b311775h

Reference yield:

: 172405-21-9
methyl N-<2-((4-methoxyphenyl)-diphenylmethyl)aminoethyl> glycinate

: 676555-67-2
[[2-(2-Amino-6-benzyloxy-purin-9-yl)-acetyl]-(2-{2-[[2-(6-benzyloxycarbonylamino-purin-9-yl)-acetyl]-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / diisopropylethylamine; bromo-tris-(dimethylamino)-phosphonium-hexafluorophosphate / dimethylformamide / 2 h / 20 °C

2: aq. LiOH / dioxane / 2 h / 20 °C

3: 91 percent / diisopropylethylamine; bromo-tris-(dimethylamino)-phosphonium-hexafluorophosphate / dimethylformamide / 0.17 h / -15 °C

With lithium hydroxide; bromo-tris-dimethylamino-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/b311775h