1,2-DIHYDROACENAPHTHYLEN-1-YLACETIC ACID

Base Information

Chemical Name:1,2-DIHYDROACENAPHTHYLEN-1-YLACETIC ACID
CAS No.:7508-18-1
Molecular Formula:C₁₄H₁₂O₂
Molecular Weight:212.248
Hs Code.:
Mol file:7508-18-1.mol

Synonyms:2-acenaphthenylacetic acid;2-(1,2-Dihydro-1-acenaphthylenyl)acetic Acid;Acenaphthyl-1-essigsaeure;1-Acenaphtheneacetic acid;1-Acenaphthenylacetic acid;acenaphthen-1-yl-acetic acid;1,2-dihydroacenaphthylen-1-ylacetic acid;Acenaphthen-1-yl-essigsaeure;

Suppliers and Price of 1,2-DIHYDROACENAPHTHYLEN-1-YLACETIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,2-DIHYDROACENAPHTHYLEN-1-YLACETIC ACID

Chemical Property:

Vapor Pressure:1.03E-08mmHg at 25°C
Boiling Point:445.4°Cat760mmHg
Flash Point:342°C
PSA：37.30000
Density:1.27g/cm³
LogP:2.95420

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2-DIHYDROACENAPHTHYLEN-1-YLACETIC ACID

There total 6 articles about 1,2-DIHYDROACENAPHTHYLEN-1-YLACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7508-18-1
1-Acenaphthenylacetic acid

Guidance literature:: at 190 ℃;
DOI:10.1021/jo50005a008 DOI:10.1021/ja01846a046

Reference yield:

: 103457-82-5
ethyl 2-(1,2-dihydroacenaphthylen-1-yl)acetate

: 7508-18-1
1-Acenaphthenylacetic acid

Guidance literature:: With potassium hydroxide; In methanol; Heating;
DOI:10.1021/jm000922c

Reference yield:

: 231949-34-1
Ethyl₂-(1,2-dihydro-1-acenaphthylenylidene)acetate

: 7508-18-1
1-Acenaphthenylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄; PdCl₂; H₂ / methanol / 2.5 h / 20 °C

2: aq. KOH / methanol / Heating

With potassium hydroxide; sodium tetrahydroborate; hydrogen; palladium dichloride; In methanol; 1: Catalytic hydrogenation / 2: Hydrolysis;
DOI:10.1021/jm000922c