Butanediamide, N-[8-(benzoylamino)octyl]-N'-[2-[2-(phenylmethoxy)-1-[(phenylmethoxy) methyl]ethoxy]-1-[[2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy] methyl]ethyl]-

Base Information

Chemical Name:Butanediamide, N-[8-(benzoylamino)octyl]-N'-[2-[2-(phenylmethoxy)-1-[(phenylmethoxy) methyl]ethoxy]-1-[[2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy] methyl]ethyl]-
CAS No.:677718-63-7
Molecular Formula:C56H71N3O9
Molecular Weight:930.194
Hs Code.:

Butanediamide,
N-[8-(benzoylamino)octyl]-N'-[2-[2-(phenylmethoxy)-1-[(phenylmethoxy)
methyl]ethoxy]-1-[[2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy]
methyl]ethyl]-

Synonyms:

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Chemical Property of Butanediamide, N-[8-(benzoylamino)octyl]-N'-[2-[2-(phenylmethoxy)-1-[(phenylmethoxy) methyl]ethoxy]-1-[[2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy] methyl]ethyl]-

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Technology Process of Butanediamide, N-[8-(benzoylamino)octyl]-N'-[2-[2-(phenylmethoxy)-1-[(phenylmethoxy) methyl]ethoxy]-1-[[2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy] methyl]ethyl]-

There total 4 articles about Butanediamide, N-[8-(benzoylamino)octyl]-N'-[2-[2-(phenylmethoxy)-1-[(phenylmethoxy) methyl]ethoxy]-1-[[2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy] methyl]ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 677718-43-3
2,5-dioxopyrrolidinyl 3-{N-[2-{2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}-1-({2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}methyl)ethyl]carbamoyl}propanoate

: 66095-35-0
N-(8-aminooctyl)benzamide

: 677718-63-7
N'-[8-(phenylcarbonylamino)octyl]-N-[2-{2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}-1-({2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}methyl)ethyl]butane-1,4-diamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1002/ejoc.200601036

Reference yield:

: 677718-40-0
3-{N-[2-{2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}-1-({2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}methyl)ethyl]carbamoyl}propanoic acid

: 677718-63-7
N'-[8-(phenylcarbonylamino)octyl]-N-[2-{2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}-1-({2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}methyl)ethyl]butane-1,4-diamide

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / triethylamine; 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide*HCl / tetrahydrofuran / Heating

2: 99 percent / triethylamine / tetrahydrofuran / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran;
DOI:10.1002/ejoc.200601036

Reference yield:

: 156536-14-0
2-amino-1,3-bis(1,3-dibenzyl-2-glyceroxy)-2-propane

: 677718-63-7
N'-[8-(phenylcarbonylamino)octyl]-N-[2-{2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}-1-({2-(phenylmethoxy)-1-[(phenylmethoxy)methyl]ethoxy}methyl)ethyl]butane-1,4-diamide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / 4 h / 100 °C

2: 77 percent / triethylamine; 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide*HCl / tetrahydrofuran / Heating

3: 99 percent / triethylamine / tetrahydrofuran / 20 °C

With pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran;
DOI:10.1002/ejoc.200601036