Technology Process of Cyclohexanone, 2,2-dimethyl-6-[4-(phenylsulfonyl)butyl]-
There total 6 articles about Cyclohexanone, 2,2-dimethyl-6-[4-(phenylsulfonyl)butyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetra-(n-butyl)ammonium iodide;
In
water; acetone; benzene;
at 110 ℃;
for 14h;
DOI:10.1248/cpb.52.132
- Guidance literature:
-
Multi-step reaction with 6 steps
1: LiAlH4 / diethyl ether / 0.25 h / 0 °C
2: DMAP; Et3N / CH2Cl2 / 3 h / 20 °C
3: 1.63 g / PDC / CH2Cl2 / 8 h
4: 98 percent / tetrabutylammonium fluoride / tetrahydrofuran / 4 h / 0 °C
5: carbon tetrabromide; triphenylphosphine / CH2Cl2 / 0.17 h / 0 °C
6: 960 mg / TBAI / H2O; acetone; benzene / 14 h / 110 °C
With
dmap; lithium aluminium tetrahydride; dipyridinium dichromate; carbon tetrabromide; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; benzene;
DOI:10.1248/cpb.52.132
- Guidance literature:
-
Multi-step reaction with 5 steps
1: DMAP; Et3N / CH2Cl2 / 3 h / 20 °C
2: 1.63 g / PDC / CH2Cl2 / 8 h
3: 98 percent / tetrabutylammonium fluoride / tetrahydrofuran / 4 h / 0 °C
4: carbon tetrabromide; triphenylphosphine / CH2Cl2 / 0.17 h / 0 °C
5: 960 mg / TBAI / H2O; acetone; benzene / 14 h / 110 °C
With
dmap; dipyridinium dichromate; carbon tetrabromide; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water; acetone; benzene;
DOI:10.1248/cpb.52.132
