rel-5-Acetyl-2-[(2R,6S)-2,6-dimethyl-4-morpholinyl]benzaldehyde

Base Information

Chemical Name:rel-5-Acetyl-2-[(2R,6S)-2,6-dimethyl-4-morpholinyl]benzaldehyde
CAS No.:679839-43-1
Molecular Formula:C15H19NO3
Molecular Weight:261.321
Hs Code.:
DSSTox Substance ID:DTXSID101174053

Synonyms:SCHEMBL1592530;DTXSID101174053;rel-5-Acetyl-2-[(2R,6S)-2,6-dimethyl-4-morpholinyl]benzaldehyde;679839-43-1

Suppliers and Price of rel-5-Acetyl-2-[(2R,6S)-2,6-dimethyl-4-morpholinyl]benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of rel-5-Acetyl-2-[(2R,6S)-2,6-dimethyl-4-morpholinyl]benzaldehyde

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:261.13649347
Heavy Atom Count:19
Complexity:334

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1CN(CC(O1)C)C2=C(C=C(C=C2)C(=O)C)C=O
Isomeric SMILES:C[C@@H]1CN(C[C@@H](O1)C)C2=C(C=C(C=C2)C(=O)C)C=O

Technology Process of rel-5-Acetyl-2-[(2R,6S)-2,6-dimethyl-4-morpholinyl]benzaldehyde

There total 2 articles about rel-5-Acetyl-2-[(2R,6S)-2,6-dimethyl-4-morpholinyl]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 914936-25-7,679839-42-0
cis-4-[4-bromo-2-(1,3-dioxolan-2-yl)phenyl]-2,6-dimethylmorpholine

: 78191-00-1
N-Methoxy-N-methylacetamide

: 679839-43-1
cis-5-acetyl-2-(2,6-dimethylmorpholin-4-yl)benzaldehyde

Guidance literature:: cis-4-[4-bromo-2-(1,3-dioxolan-2-yl)phenyl]-2,6-dimethylmorpholine; With tert.-butyl lithium; In tetrahydrofuran; hexanes; at -78 - -70 ℃; for 0.616667h;

N-Methoxy-N-methylacetamide; In tetrahydrofuran; hexanes; at -78 - 0 ℃;

With hydrogenchloride; sodium carbonate; more than 3 stages;