2,4,6,8,10,12-Tridecahexaenal, 13-[4-(hexyloxy)-3-methoxyphenyl]-3,7,11-trimethyl-, (2E,4E,6E,8E,10E,12E)-

Base Information

Chemical Name:2,4,6,8,10,12-Tridecahexaenal, 13-[4-(hexyloxy)-3-methoxyphenyl]-3,7,11-trimethyl-, (2E,4E,6E,8E,10E,12E)-
CAS No.:680575-27-3
Molecular Formula:C29H38O3
Molecular Weight:434.619
Hs Code.:

Synonyms:

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Chemical Property of 2,4,6,8,10,12-Tridecahexaenal, 13-[4-(hexyloxy)-3-methoxyphenyl]-3,7,11-trimethyl-, (2E,4E,6E,8E,10E,12E)-

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Technology Process of 2,4,6,8,10,12-Tridecahexaenal, 13-[4-(hexyloxy)-3-methoxyphenyl]-3,7,11-trimethyl-, (2E,4E,6E,8E,10E,12E)-

There total 6 articles about 2,4,6,8,10,12-Tridecahexaenal, 13-[4-(hexyloxy)-3-methoxyphenyl]-3,7,11-trimethyl-, (2E,4E,6E,8E,10E,12E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 58274-64-9,82223-93-6,73912-36-4
(E)-trimethyl((3-methylbuta-1,3-dien-1-yl)oxy)silane

: 4-((1E,3E,5E,7E)-9,9-Diethoxy-3,7-dimethyl-nona-1,3,5,7-tetraenyl)-1-hexyloxy-2-methoxy-benzene

: 680575-27-3
(2E,4E,6E,8E,10E,12E)-13-(4-hexyloxy-3-methoxyphenyl)-3,7,11-trimethyl-trideca-2,4,6,8,10,12-hexaenal

Guidance literature:: (E)-trimethyl((3-methylbuta-1,3-dien-1-yl)oxy)silane; 4-((1E,3E,5E,7E)-9,9-Diethoxy-3,7-dimethyl-nona-1,3,5,7-tetraenyl)-1-hexyloxy-2-methoxy-benzene; With zinc(II) chloride; In diethyl ether; at 5 ℃; for 36h;

With Pyridine hydrobromide; In water; acetone; at 40 ℃; Further stages.;
DOI:10.1016/j.tet.2003.12.008

Reference yield:

: 58274-64-9,82223-93-6,73912-36-4
(E)-trimethyl((3-methylbuta-1,3-dien-1-yl)oxy)silane

: 680575-27-3
(2E,4E,6E,8E,10E,12E)-13-(4-hexyloxy-3-methoxyphenyl)-3,7,11-trimethyl-trideca-2,4,6,8,10,12-hexaenal

Guidance literature:: Multi-step reaction with 5 steps

1.1: ZnCl₂ / diethyl ether / 36 h / 5 °C

1.2: 74 percent / pyridine hydrobromide / acetone; H₂O / 40 °C

2.1: camphorsulfonic acid / diethyl ether / 25 °C

3.1: ZnCl₂ / diethyl ether / 36 h / 5 °C

3.2: 68 percent / pyridine hydrobromide / acetone; H₂O / 40 °C

4.1: camphorsulfonic acid / diethyl ether / 25 °C

5.1: ZnCl₂ / diethyl ether / 36 h / 5 °C

5.2: 59 percent / pyridine hydrobromide / acetone; H₂O / 40 °C

With camphor-10-sulfonic acid; zinc(II) chloride; In diethyl ether;
DOI:10.1016/j.tet.2003.12.008

Reference yield:

: 680575-18-2
4-diethoxymethyl-1-hexyloxy-2-methoxy-benzene

: 680575-27-3
(2E,4E,6E,8E,10E,12E)-13-(4-hexyloxy-3-methoxyphenyl)-3,7,11-trimethyl-trideca-2,4,6,8,10,12-hexaenal

Guidance literature:: Multi-step reaction with 5 steps

1.1: ZnCl₂ / diethyl ether / 36 h / 5 °C

1.2: 74 percent / pyridine hydrobromide / acetone; H₂O / 40 °C

2.1: camphorsulfonic acid / diethyl ether / 25 °C

3.1: ZnCl₂ / diethyl ether / 36 h / 5 °C

3.2: 68 percent / pyridine hydrobromide / acetone; H₂O / 40 °C

4.1: camphorsulfonic acid / diethyl ether / 25 °C

5.1: ZnCl₂ / diethyl ether / 36 h / 5 °C

5.2: 59 percent / pyridine hydrobromide / acetone; H₂O / 40 °C

With camphor-10-sulfonic acid; zinc(II) chloride; In diethyl ether;
DOI:10.1016/j.tet.2003.12.008