1,5-Methano-1H-azocino[4,3-b]indol-6-ol,12-ethyl-2,3,4,5,6,7-hexahydro-2-methyl-, (1R,5R,6S,12R)- (9CI)

Base Information

• Chemical Name: 1,5-Methano-1H-azocino[4,3-b]indol-6-ol,12-ethyl-2,3,4,5,6,7-hexahydro-2-methyl-, (1R,5R,6S,12R)- (9CI)
• CAS No.: 32223-44-2
• Molecular Formula: C₁₇H₂₂N₂O
• Molecular Weight: 270.374

Synonyms:Dasycarpidan-1-ol,(1a,3R)-; 1,5-Methano-1H-azocino[4,3-b]indol-6-ol,12-ethyl-2,3,4,5,6,7-hexahydro-2-methyl-, [1R-(1a,5a,6b,12R*)]-; 3-Epidasycarpidan-1a-ol; 3-Epidasycarpidol

Chemical Property of 1,5-Methano-1H-azocino[4,3-b]indol-6-ol,12-ethyl-2,3,4,5,6,7-hexahydro-2-methyl-, (1R,5R,6S,12R)- (9CI)

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SDS file from LookChem

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Technology Process of 1,5-Methano-1H-azocino[4,3-b]indol-6-ol,12-ethyl-2,3,4,5,6,7-hexahydro-2-methyl-, (1R,5R,6S,12R)- (9CI)

There total 20 articles about 1,5-Methano-1H-azocino[4,3-b]indol-6-ol,12-ethyl-2,3,4,5,6,7-hexahydro-2-methyl-, (1R,5R,6S,12R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

6-acetoxy-12β-ethyl-2-methyl-3-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole → (+/-)-dasycarpinol (2744-46-9,32223-44-2,139973-16-3,139973-17-4)

Guidance literature:

With sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1055/s-0035-1562528

Reference yield: 24.0%

(±)-dasycarpidone (2825-08-3,16530-89-5,18688-38-5,18700-27-1) → C17H22N2O (2744-46-9,32223-44-2,139973-16-3,139973-17-4) + (+/-)-dasycarpinol (2744-46-9,32223-44-2,139973-16-3,139973-17-4)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 6h; Ambient temperature;

DOI:10.1039/c39910001687

Reference yield: 24.0%

(±)-dasycarpidone (2825-08-3,16530-89-5,18688-38-5,18700-27-1) → C17H22N2O (2744-46-9,32223-44-2,139973-16-3,139973-17-4) + (+/-)-dasycarpinol (2744-46-9,32223-44-2,139973-16-3,139973-17-4)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 6h; Ambient temperature;

DOI:10.1039/c39910001687

upstream raw materials:

(±)-dasycarpidone

C₂₃H₂₆N₂

(1RS,5RS,12SR)-12-ethyl-1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

C₂₄H₂₆N₂O₂

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