33DIACETYLAMINO22DIMETHYLAZOXYBENZENE

Base Information

• Chemical Name: 33DIACETYLAMINO22DIMETHYLAZOXYBENZENE
• CAS No.: 143922-99-0
• Molecular Formula: C₁₈H₂₀N₄O₂
• Molecular Weight: 324.382
• Mol file: 143922-99-0.mol

Synonyms:Ccris 5400

Chemical Property of 33DIACETYLAMINO22DIMETHYLAZOXYBENZENE

Chemical Property:

• Vapor Pressure: 1.44E-11mmHg at 25°C
• Boiling Point: 536.2°Cat760mmHg
• Flash Point: 278.1°C
• PSA: 89.90000
• Density: 1.17g/cm³
• LogP: 5.93460

Purity/Quality:

99%min ^*data from raw suppliers

3,3'-DIACETYLAMINO-2,2'-DIMETHYLAZOBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 33DIACETYLAMINO22DIMETHYLAZOXYBENZENE

There total 3 articles about 33DIACETYLAMINO22DIMETHYLAZOXYBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-nitro-o-tolylamine (603-83-8) → bis-(3-acetylamino-2-methyl-phenyl)-diazene (143922-99-0)

Guidance literature:

Multi-step reaction with 2 steps

1: alcohol; alcoholic tin dichloride

2: glacial acetic acid

With ethanol; acetic acid; tin(ll) chloride;

Reference yield:

o-toluidine (95-53-4) → bis-(3-acetylamino-2-methyl-phenyl)-diazene (143922-99-0)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid; HNO₃+H₂SO₄

2: alcohol; alcoholic tin dichloride

3: glacial acetic acid

With ethanol; sulfuric acid; nitric acid; acetic acid; tin(ll) chloride;

Reference yield:

bis-(3-amino-2-methyl-phenyl)-diazene (143922-97-8) + acetic anhydride (108-24-7) → bis-(3-acetylamino-2-methyl-phenyl)-diazene (143922-99-0)

Guidance literature:

With acetic acid;

upstream raw materials:

bis-(3-amino-2-methyl-phenyl)-diazene

acetic anhydride

3-nitro-o-tolylamine

o-toluidine