(5R)-3-[[(Aminocarbonyl)oxy]methyl]-6β-[(R)-1-hydroxyethyl]-7-oxo-4-thia-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid sodium salt

Base Information

Chemical Name:(5R)-3-[[(Aminocarbonyl)oxy]methyl]-6β-[(R)-1-hydroxyethyl]-7-oxo-4-thia-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid sodium salt
CAS No.:84845-58-9
Molecular Formula:C10H12N2O6S
Molecular Weight:310.2589
Hs Code.:
Mol file:84845-58-9.mol

Synonyms:Sodium;(5R,6S)-3-carbamoyloxymethyl-6-((R)-1-hydroxy-ethyl)-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylate;Sodium(5R,6S)-2-carbamoyloxymethyl-6-[1(R)-hydroxyethyl]-penem-3-carboxylate;Sodium (5R)-2-carbamoyloxymethyl-6(S)-[1(R)-hydroxyethyl]-2-penem-3-carboxylate;

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Chemical Property of (5R)-3-[[(Aminocarbonyl)oxy]methyl]-6β-[(R)-1-hydroxyethyl]-7-oxo-4-thia-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid sodium salt

Chemical Property:

Vapor Pressure:3.42E-20mmHg at 25°C
Boiling Point:659.4°Cat760mmHg
Flash Point:352.6°C
PSA：158.29000
Density:g/cm³
LogP:-1.40650

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Technology Process of (5R)-3-[[(Aminocarbonyl)oxy]methyl]-6β-[(R)-1-hydroxyethyl]-7-oxo-4-thia-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid sodium salt

There total 22 articles about (5R)-3-[[(Aminocarbonyl)oxy]methyl]-6β-[(R)-1-hydroxyethyl]-7-oxo-4-thia-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98525-49-6
{(2R,3S)-3-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-2-[2-(tert-butyl-diphenyl-silanyloxy)-acetylsulfanyl]-4-oxo-azetidin-1-yl}-oxo-acetic acid 2,2,2-trichloro-ethyl ester

: 84845-58-9
FCE 221O₁

: penem

Guidance literature:: With triethyl phosphite; In toluene; for 9h; Heating;
DOI:10.1021/ja00308a044

Reference yield:

tetrakistriphenylphosphine-Pd: tetrakistriphenylphosphine-Pd

: 96559-10-3
allyl (5R,6S)-2-carbamoyloxymethyl-6-<(1R)-1-hydroxyethyl>penem-3-carboxylate

: 84845-58-9
FCE 221O₁

Guidance literature:: With sodium; triphenylphosphine; In tetrahydrofuran;

Reference yield:

: 105455-35-4
2-{(2R,3R)-3-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-ethyl]-2-[2-(tert-butyl-diphenyl-silanyloxy)-acetylsulfanyl]-4-oxo-azetidin-1-yl}-3-methyl-but-2-enoic acid 2,2,2-trichloro-ethyl ester

: 84845-58-9
FCE 221O₁

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) O₃, 2.) Me₂S / 1.) CH₂Cl₂, -70 deg C

2: triethylphosphite / toluene / 9 h / Heating

With dimethylsulfide; ozone; triethyl phosphite; In toluene;
DOI:10.1021/ja00308a044