Technology Process of Benzene,
[[5-[2-[(phenylmethoxy)methyl]cyclopropyl]-4-pentenyl]sulfonyl]-
There total 4 articles about Benzene,
[[5-[2-[(phenylmethoxy)methyl]cyclopropyl]-4-pentenyl]sulfonyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium tert-butoxide / tetrahydrofuran / 2.25 h / 0 - 20 °C
1.2: 81 percent / tetrahydrofuran / 2 h / 0 - 10 °C
2.1: 91 percent / lithium aluminum hydride / tetrahydrofuran / 0.67 h / 0 °C
3.1: 863 mg / triethylamine; DMAP / CH2Cl2 / 12 h / 0 - 20 °C
4.1: 650 mg / Bu4NI; Cu / tetrahydrofuran / 12 h / Heating
With
dmap; lithium aluminium tetrahydride; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; copper; triethylamine;
In
tetrahydrofuran; dichloromethane;
1.2: Wittig reaction;
DOI:10.1021/jo0302760
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 863 mg / triethylamine; DMAP / CH2Cl2 / 12 h / 0 - 20 °C
2: 650 mg / Bu4NI; Cu / tetrahydrofuran / 12 h / Heating
With
dmap; tetra-(n-butyl)ammonium iodide; copper; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo0302760
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / lithium aluminum hydride / tetrahydrofuran / 0.67 h / 0 °C
2: 863 mg / triethylamine; DMAP / CH2Cl2 / 12 h / 0 - 20 °C
3: 650 mg / Bu4NI; Cu / tetrahydrofuran / 12 h / Heating
With
dmap; lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; copper; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo0302760
