Glycine, N-[2-(1,1-dimethylethoxy)-2-oxoethyl]-N-[2-[[2-[[2-(1,1-dimethylethoxy)-2 -oxoethyl]thio]phenyl]amino]-2-oxoethyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Glycine, N-[2-(1,1-dimethylethoxy)-2-oxoethyl]-N-[2-[[2-[[2-(1,1-dimethylethoxy)-2 -oxoethyl]thio]phenyl]amino]-2-oxoethyl]-, 1,1-dimethylethyl ester
CAS No.:681430-42-2
Molecular Formula:C₂₆H₄₀N₂O₇S
Molecular Weight:524.679
Hs Code.:

Glycine,
N-[2-(1,1-dimethylethoxy)-2-oxoethyl]-N-[2-[[2-[[2-(1,1-dimethylethoxy)-2
-oxoethyl]thio]phenyl]amino]-2-oxoethyl]-, 1,1-dimethylethyl ester

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Chemical Property of Glycine, N-[2-(1,1-dimethylethoxy)-2-oxoethyl]-N-[2-[[2-[[2-(1,1-dimethylethoxy)-2 -oxoethyl]thio]phenyl]amino]-2-oxoethyl]-, 1,1-dimethylethyl ester

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Technology Process of Glycine, N-[2-(1,1-dimethylethoxy)-2-oxoethyl]-N-[2-[[2-[[2-(1,1-dimethylethoxy)-2 -oxoethyl]thio]phenyl]amino]-2-oxoethyl]-, 1,1-dimethylethyl ester

There total 2 articles about Glycine, N-[2-(1,1-dimethylethoxy)-2-oxoethyl]-N-[2-[[2-[[2-(1,1-dimethylethoxy)-2 -oxoethyl]thio]phenyl]amino]-2-oxoethyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137-07-5
2-amino-benzenethiol

: 681430-42-2
di-tert-butyl N-[N-o-(tert-butoxycarbonylmethylsulfanyl)phenylcarbamoylmethyl]iminodiacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 76 percent / K₂CO₃; KI / tetrahydrofuran / 18 h / 60 °C

2.1: oxalyl chloride; DMF / tetrahydrofuran / 0 - 20 °C

2.2: 93 percent / iPr₂EtN / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

3.1: H₂; piperidine / CH₂Cl₂ / 0.33 h

3.2: 75 percent / K₂CO₃; KI / tetrahydrofuran / 5 h / 70 °C

With piperidine; oxalyl dichloride; hydrogen; potassium carbonate; N,N-dimethyl-formamide; potassium iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200300459

Reference yield:

: 681430-37-5
tert-butyl o-aminophenylsulfanyl acetate

: 681430-42-2
di-tert-butyl N-[N-o-(tert-butoxycarbonylmethylsulfanyl)phenylcarbamoylmethyl]iminodiacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl chloride; DMF / tetrahydrofuran / 0 - 20 °C

1.2: 93 percent / iPr₂EtN / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

2.1: H₂; piperidine / CH₂Cl₂ / 0.33 h

2.2: 75 percent / K₂CO₃; KI / tetrahydrofuran / 5 h / 70 °C

With piperidine; oxalyl dichloride; hydrogen; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200300459