Technology Process of 2,4,8,10,12,14-Pentadecahexaen-6-ynal,4,9,13-trimethyl-15-(2,6,6-trimethyl-1-cyclohexen-1-yl)-,(2E,4E,8E,10E,12E,14E)-
There total 3 articles about 2,4,8,10,12,14-Pentadecahexaen-6-ynal,4,9,13-trimethyl-15-(2,6,6-trimethyl-1-cyclohexen-1-yl)-,(2E,4E,8E,10E,12E,14E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
phosphoric acid; toluene-4-sulfonic acid;
Behandeln des Reaktionsprodukts mit Aethyl-vinyl-aether und ZnCl2 in Aethylacetat und Erwaermen des danach erhaltenen Reaktionsprodukts mit Essigsaeure und Natriumacetat;
DOI:10.1002/hlca.19590420328
- Guidance literature:
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1,1,3-Triethoxy-4-methyl-hept-4-en-6-in, 1) Ethylmagnesiumbromid, Ae., 2) β-C(19)-Aldehyd, 3) ethanol. HCl;
- Guidance literature:
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13-(2,6,6-Trimethyl-cyclohex-1-enyl)-2,7,11-trimethyl-1,1-diethoxy-tridec-2,6,8,8,10,12-pentan-4-in, 1.) Vinyl-ethyl-ether, 2.) Saeure;