{2-[(2-Nitrophenyl)sulfanyl]phenyl}hydrazine

Base Information

Chemical Name:{2-[(2-Nitrophenyl)sulfanyl]phenyl}hydrazine
CAS No.:68207-43-2
Molecular Formula:C12H11N3O2S
Molecular Weight:261.304
Hs Code.:
DSSTox Substance ID:DTXSID20499391
Wikidata:Q82350129

Synonyms:68207-43-2;{2-[(2-Nitrophenyl)sulfanyl]phenyl}hydrazine;DTXSID20499391

Suppliers and Price of {2-[(2-Nitrophenyl)sulfanyl]phenyl}hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of {2-[(2-Nitrophenyl)sulfanyl]phenyl}hydrazine

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:261.05719778
Heavy Atom Count:18
Complexity:285

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)NN)SC2=CC=CC=C2[N+](=O)[O-]

Technology Process of {2-[(2-Nitrophenyl)sulfanyl]phenyl}hydrazine

There total 3 articles about {2-[(2-Nitrophenyl)sulfanyl]phenyl}hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 19284-81-2
2-(2-nitro)phenylthiophenylamine

: 68207-43-2
{2-[(2-nitrophenyl)thio]phenyl}hydrazine

Guidance literature:: 2-(2-nitro)phenylthiophenylamine; With hydrogenchloride; In water; at 20 ℃; for 2h;

With sodium nitrite; In water; at 0 - 5 ℃; for 1h; Further stages;
DOI:10.1016/j.ejmech.2011.03.003

Reference yield:

: 88-73-3
2-Chloronitrobenzene

: 68207-43-2
{2-[(2-nitrophenyl)thio]phenyl}hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 5 h / Reflux

2.1: hydrogenchloride / water / 2 h / 20 °C

2.2: 1 h / 0 - 5 °C

With hydrogenchloride; potassium hydroxide; In ethanol; water;
DOI:10.1016/j.ejmech.2011.03.003