Phosphoric acid, diethyl 3-(4-fluorophenyl)-2-propenyl ester

Base Information

Chemical Name:Phosphoric acid, diethyl 3-(4-fluorophenyl)-2-propenyl ester
CAS No.:682339-14-6
Molecular Formula:C13H18FO4P
Molecular Weight:288.256
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphoric acid, diethyl 3-(4-fluorophenyl)-2-propenyl ester

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Technology Process of Phosphoric acid, diethyl 3-(4-fluorophenyl)-2-propenyl ester

There total 1 articles about Phosphoric acid, diethyl 3-(4-fluorophenyl)-2-propenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124980-95-6,7361-55-9
3-(4-fluorophenyl)prop-2-en-1-ol

: 814-49-3
diethyl chlorophosphate

: 682339-14-6
C₁₃H₁₈FO₄P

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 - 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.5b03692

Reference yield: 88.0%

: 682339-14-6
C₁₃H₁₈FO₄P

: 78782-17-9
4,4,5,5-tetramethyl-2-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]-1,3,2-dioxaborolane

: 2-(2-(4-fluorophenyl)but-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 4,4,5,5-tetramethyl-2-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]-1,3,2-dioxaborolane; With C₁₃H₁₉N₂O⁽¹⁺⁾*Cl^(1-); lithium methanolate; copper(l) chloride; In 1,4-dioxane; at 60 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

C₁₃H₁₈FO₄P; In 1,4-dioxane; at 60 ℃; for 24h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.5b03692

Reference yield: 75.0%

: 682339-14-6
C₁₃H₁₈FO₄P

: 2,2'-(ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 2-(3-(4-fluorophenyl)pent-4-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: C₁₇H₂₄BFO₂

Guidance literature:: 2,2'-(ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane); With C₁₉H₂₂ClCuN₂; lithium methanolate; In tetrahydrofuran; at 60 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

C₁₃H₁₈FO₄P; In tetrahydrofuran; at 60 ℃; for 24h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.5b03692