Phosphoric acid, 3-(3-chlorophenyl)-2-propenyl diethyl ester

Base Information

Chemical Name:Phosphoric acid, 3-(3-chlorophenyl)-2-propenyl diethyl ester
CAS No.:682339-16-8
Molecular Formula:C13H18ClO4P
Molecular Weight:304.71
Hs Code.:

Synonyms:

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Chemical Property of Phosphoric acid, 3-(3-chlorophenyl)-2-propenyl diethyl ester

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Technology Process of Phosphoric acid, 3-(3-chlorophenyl)-2-propenyl diethyl ester

There total 1 articles about Phosphoric acid, 3-(3-chlorophenyl)-2-propenyl diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1504-67-2
3-(3-chlorophenyl)prop-2-en-1-ol

: 814-49-3
diethyl chlorophosphate

: 682339-16-8
C₁₃H₁₈ClO₄P

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 - 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.5b03692

Reference yield: 77.0%

: 682339-16-8
C₁₃H₁₈ClO₄P

: 78782-17-9
4,4,5,5-tetramethyl-2-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]-1,3,2-dioxaborolane

: 2-(2-(3-chlorophenyl)but-3-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 4,4,5,5-tetramethyl-2-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]-1,3,2-dioxaborolane; With C₁₃H₁₉N₂O⁽¹⁺⁾*Cl^(1-); lithium methanolate; copper(l) chloride; In 1,4-dioxane; at 60 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

C₁₃H₁₈ClO₄P; In 1,4-dioxane; at 60 ℃; for 24h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.5b03692

Reference yield:

: 682339-16-8
C₁₃H₁₈ClO₄P

: 932-90-1
Benzaldoxime

: (E)-O-[3-(3-chlorophenyl)prop-2-enyl]benzaldehyde oxime

: 1167995-00-7
(E)-O-[(S)-1-(3-chlorophenyl)prop-2-enyl]benzaldehyde oxime

Guidance literature:: Benzaldoxime; With barium hydroxide monohydrate; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

C₁₃H₁₈ClO₄P; With bis(1,5-cyclooctadiene)diiridium(I) dichloride; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine; In dichloromethane; at -20 ℃; for 40h; optical yield given as %ee; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.04.005