5H-Dibenzo[b,e]azepine-6,11-dione

Base Information

• Chemical Name: 5H-Dibenzo[b,e]azepine-6,11-dione
• CAS No.: 1143-50-6
• Molecular Formula: C14H9NO2
• Molecular Weight: 223.231
• Hs Code.: 2933990090
• European Community (EC) Number: 214-539-6
• NSC Number: 144965
• UNII: T0WI39HQ1R
• DSSTox Substance ID: DTXSID80150693
• Nikkaji Number: J203.399B
• Wikidata: Q72463440
• ChEMBL ID: CHEMBL242201
• Mol file: 1143-50-6.mol

Synonyms:5H-dibenzo(b,e)azepine-6,11-dione

Chemical Property of 5H-Dibenzo[b,e]azepine-6,11-dione

Chemical Property:

• Vapor Pressure: 0.000204mmHg at 25°C
• Melting Point: 245-246 °C
• Refractive Index: 1.636
• Boiling Point: 327.3 °C at 760 mmHg
• PKA: 12.43±0.20(Predicted)
• Flash Point: 131.3 °C
• PSA: 49.93000
• Density: 1.291 g/cm³
• LogP: 2.04150
• Storage Temp.: Sealed in dry,Room Temperature
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 223.063328530
• Heavy Atom Count: 17
• Complexity: 339

Purity/Quality:

98% ^*data from raw suppliers

5H-Dibenzo(b,e)azepine-6,11-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C(=O)C3=CC=CC=C3NC2=O

Technology Process of 5H-Dibenzo[b,e]azepine-6,11-dione

There total 13 articles about 5H-Dibenzo[b,e]azepine-6,11-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

9,10-phenanthrenequinone (84-65-1) → 5,6-dihydro-6,11-dioxomorphanthridine (1143-50-6)

Guidance literature:

With sodium azide; sulfuric acid; In dichloromethane; at 0 - 20 ℃;

Reference yield: 73.0%

phthalanilic acid (4727-29-1) → 5,6-dihydro-6,11-dioxomorphanthridine (1143-50-6)

Guidance literature:

With PPA; at 95 - 100 ℃;

DOI:10.1081/SCC-120004842

Reference yield: 72.0%

anthracen-9(10H)-one (90-44-8) → 5,6-dihydro-6,11-dioxomorphanthridine (1143-50-6)

Guidance literature:

With trimethylsilylazide; diphenyl phosphoryl azide; water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride; In trifluoroacetic acid; at 100 ℃; for 96h; Inert atmosphere;

DOI:10.1002/anie.201106112

upstream raw materials:

N-phenylphthalimide

2-Benzoylbenzoic acid

2-(2-aminobenzoyl)benzoic acid

9,10-phenanthrenequinone

Downstream raw materials:

C₁₉H₂₃N₃O₃

N-<3-Dimethylamino-propyl>-homoacridan

N-(2-Diethylamino-ethyl)-homoacridan

C₅₆H₆₇N₁₁O₁₀

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1143-50-6 5H-DIBENZO(B,E)AZEPINE-6,11-DIONE

Send

Send

Metric Ton KG G Pound L ML

Send

Send