Benzenemethanol, 3-chloro-2-hydroxy-5-(1,1,3,3-tetramethylbutyl)-

Base Information

Chemical Name:Benzenemethanol, 3-chloro-2-hydroxy-5-(1,1,3,3-tetramethylbutyl)-
CAS No.:16372-99-9
Molecular Formula:C₁₅H₂₃ClO₂
Molecular Weight:270.799
Hs Code.:
DSSTox Substance ID:DTXSID5066039
Nikkaji Number:J421.962G
Wikidata:Q81992613
Mol file:16372-99-9.mol

Synonyms:16372-99-9;Benzenemethanol, 3-chloro-2-hydroxy-5-(1,1,3,3-tetramethylbutyl)-;2-chloro-6-(hydroxymethyl)-4-(2,4,4-trimethylpentan-2-yl)phenol;3-Chloro-2-hydroxy-5-(1,1,3,3-tetramethylbutyl)benzenemethanol;SCHEMBL7914494;DTXSID5066039;C15-H23-Cl-O2;Benzyl alcohol, 3-chloro-2-hydroxy-5-(1,1,3,3-tetramethylbutyl)-;2-Chloro-4-(1,1,3,3-tetramethylbutyl)-6-(hydroxymethyl)phenol

Suppliers and Price of Benzenemethanol, 3-chloro-2-hydroxy-5-(1,1,3,3-tetramethylbutyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Benzenemethanol, 3-chloro-2-hydroxy-5-(1,1,3,3-tetramethylbutyl)-

Chemical Property:

Vapor Pressure:3.78E-05mmHg at 25°C
Boiling Point:342.5°Cat760mmHg
Flash Point:160.9°C
PSA：40.46000
Density:1.099g/cm³
LogP:4.25170
XLogP3:5.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:270.1386577
Heavy Atom Count:18
Complexity:270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)CC(C)(C)C1=CC(=C(C(=C1)Cl)O)CO

Technology Process of Benzenemethanol, 3-chloro-2-hydroxy-5-(1,1,3,3-tetramethylbutyl)-

There total 3 articles about Benzenemethanol, 3-chloro-2-hydroxy-5-(1,1,3,3-tetramethylbutyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.3%

: 702660-37-5
2-hydroxy-3-chloro-5-(1,1,3,3-tetramethylbutyl)benzaldehyde

: 16372-99-9
2-hydroxymethyl-6-chloro-4-(1,1,3,3-tetramethylbutyl)phenol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 16h;
DOI:10.1016/j.chemphyslip.2003.08.004

Reference yield:

: 17199-24-5
2-chloro-4-(1,1,3,3-tetramethylbutyl)phenol

: 16372-99-9
2-hydroxymethyl-6-chloro-4-(1,1,3,3-tetramethylbutyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethylmagnesium bromide / diethyl ether / 16 h / 20 °C

1.2: 83.1 percent / hexamethylphosphoramide / benzene / 6 h / Heating

2.1: 77.3 percent / sodium borohydride / methanol / 16 h / 0 - 20 °C

With sodium tetrahydroborate; ethylmagnesium bromide; In methanol; diethyl ether;
DOI:10.1016/j.chemphyslip.2003.08.004

Reference yield:

: 140-66-9
tert-octylphenol

: 16372-99-9
2-hydroxymethyl-6-chloro-4-(1,1,3,3-tetramethylbutyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 96 percent / chlorine / CCl₄ / 4 h / 20 °C

2.1: ethylmagnesium bromide / diethyl ether / 16 h / 20 °C

2.2: 83.1 percent / hexamethylphosphoramide / benzene / 6 h / Heating

3.1: 77.3 percent / sodium borohydride / methanol / 16 h / 0 - 20 °C

With sodium tetrahydroborate; ethylmagnesium bromide; chlorine; In methanol; tetrachloromethane; diethyl ether;
DOI:10.1016/j.chemphyslip.2003.08.004