1,1-Cyclopropanedicarboxylic acid, 2-ethenyl-, ethyl 4-[(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)oxy]phenyl ester

Base Information

Chemical Name:1,1-Cyclopropanedicarboxylic acid, 2-ethenyl-, ethyl 4-[(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)oxy]phenyl ester
CAS No.:683795-09-7
Molecular Formula:C₂₃H₁₉F₁₃O₅
Molecular Weight:622.38
Hs Code.:

Synonyms:

Suppliers and Price of 1,1-Cyclopropanedicarboxylic acid, 2-ethenyl-, ethyl 4-[(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)oxy]phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,1-Cyclopropanedicarboxylic acid, 2-ethenyl-, ethyl 4-[(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)oxy]phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,1-Cyclopropanedicarboxylic acid, 2-ethenyl-, ethyl 4-[(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)oxy]phenyl ester

There total 5 articles about 1,1-Cyclopropanedicarboxylic acid, 2-ethenyl-, ethyl 4-[(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)oxy]phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28465-22-7
2-vinylcyclopropane-1,1-dicarboxylic acid monoethyl ester

: 683795-22-4
(2-perfluorohexyl)ethoxy-4-hydroxybenzene

: 683795-09-7
2-vinyl-cyclopropane-1,1-dicarboxylic acid ethyl ester 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyloxy)-phenyl ester

Guidance literature:: With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 50h;
DOI:10.1016/j.jfluchem.2003.07.010

Reference yield:

: 7686-78-4
diethyl 2-vinylcyclopropane-1,1-dicarboxylate

: 683795-09-7
2-vinyl-cyclopropane-1,1-dicarboxylic acid ethyl ester 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyloxy)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / KOH / ethanol / 12 h / 20 °C

2: N,N'-dicyclohexylcarbodiimide; 4-pyrrolidinopyridine / CH₂Cl₂ / 50 h / 0 - 20 °C

With potassium hydroxide; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1016/j.jfluchem.2003.07.010

Reference yield:

: 2444-19-1
4-hydroxyphenyl benzoate

: 683795-09-7
2-vinyl-cyclopropane-1,1-dicarboxylic acid ethyl ester 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyloxy)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 15 percent / PPh₃; DEAD / diethyl ether / 97 h / 20 °C

2: 97 percent / aq. KOH / ethanol / 7 h / Heating

3: N,N'-dicyclohexylcarbodiimide; 4-pyrrolidinopyridine / CH₂Cl₂ / 50 h / 0 - 20 °C

With potassium hydroxide; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; triphenylphosphine; diethylazodicarboxylate; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/j.jfluchem.2003.07.010