Acetic acid, dichloro-, 2-[1-[4-[(5S)-5-[(acetylamino)methyl]-2-oxo-3-oxazolidinyl]-2-fluorophen yl]-4-piperidinylidene]-1-methylethyl ester

Base Information

• Chemical Name: Acetic acid, dichloro-, 2-[1-[4-[(5S)-5-[(acetylamino)methyl]-2-oxo-3-oxazolidinyl]-2-fluorophen yl]-4-piperidinylidene]-1-methylethyl ester
• CAS No.: 685570-95-0
• Molecular Formula: C22H26Cl2FN3O5
• Molecular Weight: 502.37

Synonyms:

Chemical Property of Acetic acid, dichloro-, 2-[1-[4-[(5S)-5-[(acetylamino)methyl]-2-oxo-3-oxazolidinyl]-2-fluorophen yl]-4-piperidinylidene]-1-methylethyl ester

Chemical Property:

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Technology Process of Acetic acid, dichloro-, 2-[1-[4-[(5S)-5-[(acetylamino)methyl]-2-oxo-3-oxazolidinyl]-2-fluorophen yl]-4-piperidinylidene]-1-methylethyl ester

There total 1 articles about Acetic acid, dichloro-, 2-[1-[4-[(5S)-5-[(acetylamino)methyl]-2-oxo-3-oxazolidinyl]-2-fluorophen yl]-4-piperidinylidene]-1-methylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

dichloroacethyl chloride (79-36-7) + N-[[(5S)-3-[3-fluoro-4-(4-(2-hydroxy-propylidene)-piperidinyl)-phenyl]-2-oxo-5-oxazolidinyl]-methyl]-acetamide (685570-92-7) → N-[[(5S)-3-[3-fluoro-4-(4-(2-(dichloroacetoxy)-propylidene)-piperidinyl)-phenyl]-2-oxo-5-oxazolidinyl]-methyl]-acetamide (685570-95-0)

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

N-[[(5S)-3-[3-fluoro-4-(4-(2-(dichloroacetoxy)-propylidene)-piperidinyl)-phenyl]-2-oxo-5-oxazolidinyl]-methyl]-acetamide (685570-95-0) → N-[[(5S)-3-[3-fluoro-4-(4-(2-(dichloroacetoxy)-propylidene)-piperidinyl)-phenyl]-2-oxo-5-oxazolidinyl]-methyl]-acetamide hydrochloride salt (685571-19-1)

Guidance literature:

With hydrogenchloride; In diethyl ether;

upstream raw materials:

dichloroacethyl chloride

N-[[(5S)-3-[3-fluoro-4-(4-(2-hydroxy-propylidene)-piperidinyl)-phenyl]-2-oxo-5-oxazolidinyl]-methyl]-acetamide

Downstream raw materials:

N-[[(5S)-3-[3-fluoro-4-(4-(2-(dichloroacetoxy)-propylidene)-piperidinyl)-phenyl]-2-oxo-5-oxazolidinyl]-methyl]-acetamide hydrochloride salt

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