1,4-Bis(2-triphenylsilylethynyl)cyclohexane-1,4-diol

Base Information

Chemical Name:1,4-Bis(2-triphenylsilylethynyl)cyclohexane-1,4-diol
CAS No.:7224-93-3
Molecular Formula:C₂₄H₂₁NO₂
Molecular Weight:355.436
Hs Code.:
DSSTox Substance ID:DTXSID70411861
Nikkaji Number:J1.715.105C,J1.715.107J

Synonyms:7224-93-3;1,4-bis(2-triphenylsilylethynyl)cyclohexane-1,4-diol;DTXSID70411861

Suppliers and Price of 1,4-Bis(2-triphenylsilylethynyl)cyclohexane-1,4-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,4-Bis(2-triphenylsilylethynyl)cyclohexane-1,4-diol

Chemical Property:

Vapor Pressure:5.82E-23mmHg at 25°C
Boiling Point:739.5°Cat760mmHg
Flash Point:401°C
Density:1.21g/cm³
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:10
Exact Mass:680.25668358
Heavy Atom Count:50
Complexity:1010

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(CCC1(C#C[Si](C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4)O)(C#C[Si](C5=CC=CC=C5)(C6=CC=CC=C6)C7=CC=CC=C7)O

Technology Process of 1,4-Bis(2-triphenylsilylethynyl)cyclohexane-1,4-diol

There total 1 articles about 1,4-Bis(2-triphenylsilylethynyl)cyclohexane-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7224-91-1
2-(6-benzyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-ylmethyl)-aniline

: 7224-93-3
7-benzyl-6,7,7a,8-tetrahydro-5H-benzo[g][1,3]dioxolo[4',5':4,5]benzo[1,2,3-de]quinoline

Guidance literature:: Multistep reaction; (i) aq. NaNO₂, H₂SO₄, AcOH, (ii) CuCl, Cu, NH₂SO₃H, acetone;
DOI:10.1021/jo01342a507

Reference yield:

: 7224-93-3
7-benzyl-6,7,7a,8-tetrahydro-5H-benzo[g][1,3]dioxolo[4',5':4,5]benzo[1,2,3-de]quinoline

: 475-75-2
liriodenine

Guidance literature:: Multi-step reaction with 2 steps

1: Pd-C / ethanol; aq. HCl

2: O₂ / 2-methyl-propan-2-ol

With oxygen; palladium on activated charcoal; In hydrogenchloride; ethanol; tert-butyl alcohol;
DOI:10.1021/jo01342a507