Benzenemethanol, 2-(diphenylphosphinyl)-

Base Information

Chemical Name:Benzenemethanol, 2-(diphenylphosphinyl)-
CAS No.:68718-89-8
Molecular Formula:C19H17O2P
Molecular Weight:308.317
Hs Code.:
DSSTox Substance ID:DTXSID60395146
Wikidata:Q82195018

Synonyms:68718-89-8;(2-(Hydroxymethyl)phenyl)diphenylphosphine oxide;Benzenemethanol, 2-(diphenylphosphinyl)-;o-diphenylphosphinylbenzyl alcohol;DTXSID60395146;STK372976;[2-(diphenylphosphoryl)phenyl]methanol;AKOS005447061

Suppliers and Price of Benzenemethanol, 2-(diphenylphosphinyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzenemethanol, 2-(diphenylphosphinyl)-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:308.09661678
Heavy Atom Count:22
Complexity:361

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=O)(C2=CC=CC=C2)C3=CC=CC=C3CO

Technology Process of Benzenemethanol, 2-(diphenylphosphinyl)-

There total 7 articles about Benzenemethanol, 2-(diphenylphosphinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 81073-06-5
((2-hydroxymethyl)phenyl)diphenylphosphine

: 68718-89-8
(2-(hydroxymethyl)phenyl)diphenylphosphine oxide

Guidance literature:: With dihydrogen peroxide; In acetone;
DOI:10.1039/DT9930002781

Reference yield: 35.0%

: 6840-26-2
diphenyl-o-tolyl-phosphine oxide

: 68718-89-8
(2-(hydroxymethyl)phenyl)diphenylphosphine oxide

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 - 20 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2015.12.043

Reference yield:

: 144467-77-6
2-iodobenzyl diphenylphosphinite

: 68718-89-8
(2-(hydroxymethyl)phenyl)diphenylphosphine oxide

Guidance literature:: With tert.-butyl lithium; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) THF, -78 deg C, 10 min, 2.) AcOEt, 30 min;
DOI:10.1021/ja961375g