Benzamide, 3-methyl-N-[(phenylamino)thioxomethyl]-

Base Information

Chemical Name:Benzamide, 3-methyl-N-[(phenylamino)thioxomethyl]-
CAS No.:56437-99-1
Molecular Formula:C15H14N2OS
Molecular Weight:270.355
Hs Code.:
NSC Number:131948
DSSTox Substance ID:DTXSID00971867
Nikkaji Number:J140.391E
Mol file:56437-99-1.mol

Synonyms:Benzamide, 3-methyl-N-[(phenylamino)thioxomethyl]-;56437-99-1;NSC131948;3-methyl-N-(phenylcarbamothioyl)benzamide;DTXSID00971867;VRLICESMUXZLLY-UHFFFAOYSA-N;STK029312;AKOS002741409;NSC-131948;1-(3-Methylbenzoyl)-3-phenyl(thiourea);N-(3-Methylbenzoyl)-N'-phenylthiourea #;3-Methyl-N-[(phenylimino)(sulfanyl)methyl]benzene-1-carboximidic acid

Suppliers and Price of Benzamide, 3-methyl-N-[(phenylamino)thioxomethyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Benzamide, 3-methyl-N-[(phenylamino)thioxomethyl]-

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：73.22000
Density:1.258g/cm³
LogP:3.58570
XLogP3:3.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:270.08268425
Heavy Atom Count:19
Complexity:326

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)C(=O)NC(=S)NC2=CC=CC=C2

Technology Process of Benzamide, 3-methyl-N-[(phenylamino)thioxomethyl]-

There total 5 articles about Benzamide, 3-methyl-N-[(phenylamino)thioxomethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 28115-86-8
3-methylbenzoyl isothiocyanate

: 62-53-3
aniline

: 56437-99-1
N-<3-Methyl-benzoyl->-N'-phenyl-thioharnstoff

Guidance literature:: In acetone; for 1h; Heating;
DOI:10.1007/s00044-007-9017-8

Reference yield:

: 1711-06-4
3-Methylbenzoyl chloride

: 56437-99-1
N-<3-Methyl-benzoyl->-N'-phenyl-thioharnstoff

Guidance literature:: Multi-step reaction with 2 steps

1: polyethylene glycol-400; DMF / CHCl₃ / 0.17 h / Heating; microwave irradiation

2: polyethylene glycol-400; DMF / CHCl₃ / 0.07 h / Irradiation

With polyethylene glycol-400; N,N-dimethyl-formamide; In chloroform;
DOI:10.1081/SCC-120001519

Reference yield:

: 1711-06-4
3-Methylbenzoyl chloride

: 56437-99-1
N-<3-Methyl-benzoyl->-N'-phenyl-thioharnstoff

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / tetrabutylammonium bromide / benzene; H₂O / 2 h / Ambient temperature

2: benzene / 1 h / 50 °C

With tetrabutylammomium bromide; In water; benzene;