azepane-1-carbothioamide

Base Information

• Chemical Name: azepane-1-carbothioamide
• CAS No.: 68881-66-3
• Molecular Formula: C₇H₁₄N₂S
• Molecular Weight: 158.268
• Hs Code.: 2933990090
• Mol file: 68881-66-3.mol

Synonyms:azepane-1-carbothioic acid amide;1-thiocarbamoylhexahydroazepine;

Chemical Property of azepane-1-carbothioamide

Chemical Property:

• Vapor Pressure: 0.015mmHg at 25°C
• Boiling Point: 256.9oC at 760 mmHg
• Flash Point: 109.2oC
• PSA: 65.89000
• Density: 1.118g/cm3
• LogP: 1.76460

Purity/Quality:

97% purity ^*data from raw suppliers

azepane-1-carbothioamide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 25
• Safety Statements: 45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of azepane-1-carbothioamide

There total 3 articles about azepane-1-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

hexahydroazepin-1-yl cianide (5321-89-1) → 1-thiocarbamoylhexahydroazepine (68881-66-3)

Guidance literature:

Reference yield:

hexamethylene imine (111-49-9) → 1-thiocarbamoylhexahydroazepine (68881-66-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent

2: 79 percent

Reference yield:

→ 1-thiocarbamoylhexahydroazepine (68881-66-3)

Guidance literature:

entspr.t-Butylverb.4b, HCl;

upstream raw materials:

hexahydroazepin-1-yl cianide

hexamethylene imine

Downstream raw materials:

1-hexahydroazepine

5-acetyl-2-(hexahydroazepin-1-yl)-4-phenylthiazole

[2-Azepan-1-yl-4-(4-nitro-phenyl)-thiazol-5-yl]-(4-methoxy-phenyl)-methanone

1-(5-benzoyl-4-phenylthiazol-2-yl)hexahydroazepine

Refernces