1-Oxo-2-(quinolin-2-yl)-1lambda~5~-quinoline

Base Information

• Chemical Name: 1-Oxo-2-(quinolin-2-yl)-1lambda~5~-quinoline
• CAS No.: 6907-48-8
• Molecular Formula: C18H12N2O
• Molecular Weight: 272.306
• DSSTox Substance ID: DTXSID90539879
• Nikkaji Number: J645.658H
• Wikidata: Q82415694

Synonyms:2,2-biquinoline N-oxide;6907-48-8;DTXSID90539879;1-Oxo-2-(quinolin-2-yl)-1lambda~5~-quinoline

Chemical Property of 1-Oxo-2-(quinolin-2-yl)-1lambda~5~-quinoline

Chemical Property:

• XLogP3: 3.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 272.094963011
• Heavy Atom Count: 21
• Complexity: 361

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC(=N2)C3=[N+](C4=CC=CC=C4C=C3)[O-]

Technology Process of 1-Oxo-2-(quinolin-2-yl)-1lambda~5~-quinoline

There total 1 articles about 1-Oxo-2-(quinolin-2-yl)-1lambda~5~-quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

Quinoline N-oxide (1613-37-2) → 2,2'-biquinoline (119-91-5) + 2,2’-biquinoline N-oxide (6907-48-8)

Guidance literature:

With potassium hydroxide; In toluene; for 12h; Reflux; Irradiation;

DOI:10.1002/adsc.201700931

Reference yield: 87.0%

2,2’-biquinoline N-oxide (6907-48-8) → 2,2'-biquinoline (119-91-5)

Guidance literature:

With lithium tetrafluoroborate; In water; acetonitrile; at 20 ℃; for 4h; Electrochemical reaction; Inert atmosphere;

DOI:10.1002/ejoc.202000377

Reference yield: 69.0%

2,2’-biquinoline N-oxide (6907-48-8) + diphenyl acetylene (501-65-5) → 6,7-diphenyldibenzo[b,j][1,10]phenanthroline

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; Trimethylacetic acid; In 1,2-dichloro-ethane; at 120 ℃; for 18h;

DOI:10.1021/acs.orglett.8b01434

upstream raw materials:

Quinoline N-oxide

Downstream raw materials:

2,2'-biquinoline

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