2-Heptanone, 7-hydroxy-6-methyl-

Base Information

Chemical Name:2-Heptanone, 7-hydroxy-6-methyl-
CAS No.:69320-11-2
Molecular Formula:C8H16O2
Molecular Weight:144.214
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Heptanone, 7-hydroxy-6-methyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Heptanone, 7-hydroxy-6-methyl-

There total 1 articles about 2-Heptanone, 7-hydroxy-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29021-98-5
3-(2-methyl-[1,3]dioxolan-2-yl)-propan-1-ol

: 69320-11-2
6-oxo-2-methyl-1-heptanol

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / pyridinium chlorochromate, sodium acetate / CH₂Cl₂ / 0.75 h / 25 °C

2: 1.) sodium hydride / 1.) ether, 25 deg C, 45 min, 2.) 3 h

3: 98 percent / hydrogen / 5percent Pd-C / methanol / 12 h / 25 °C

4: 93 percent / lithium aluminum hydride / diethyl ether / 2 h / 0 °C

5: 86 percent / hydrochloric acid / diethyl ether / 3 h / 25 °C

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium acetate; sodium hydride; pyridinium chlorochromate; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane;

Reference yield: 97.0%

: 69320-11-2
6-oxo-2-methyl-1-heptanol

: 98-59-9
p-toluenesulfonyl chloride

: 119125-42-7
Toluene-4-sulfonic acid 2-methyl-6-oxo-heptyl ester

Guidance literature:: With pyridine;

Reference yield:

: 69320-11-2
6-oxo-2-methyl-1-heptanol

: 10408-15-8
6-methylhept-6-en-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / pyridine

2: 1.) sodium iodide, 2.) DBU / 1.) DMF, 50 deg C, 3.5 h, 2.) 80 deg C, 3.5 h

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide;