2-[(3-Nitrophenyl)methylidene]butanoyl chloride

Base Information

Chemical Name:2-[(3-Nitrophenyl)methylidene]butanoyl chloride
CAS No.:69693-44-3
Molecular Formula:C11H10ClNO3
Molecular Weight:239.658
Hs Code.:
DSSTox Substance ID:DTXSID80709882

Synonyms:2-[(3-Nitrophenyl)methylidene]butanoyl chloride;69693-44-3;DTXSID80709882

Suppliers and Price of 2-[(3-Nitrophenyl)methylidene]butanoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-[(3-Nitrophenyl)methylidene]butanoyl chloride

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:239.0349209
Heavy Atom Count:16
Complexity:309

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=CC1=CC(=CC=C1)[N+](=O)[O-])C(=O)Cl

Technology Process of 2-[(3-Nitrophenyl)methylidene]butanoyl chloride

There total 1 articles about 2-[(3-Nitrophenyl)methylidene]butanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124525-55-9
α-ethyl-m-nitrocinnamic acid

: 69693-44-3
α-ethyl-m-nitrocinnamic acid chloride

Guidance literature:: With phosphorus pentachloride; In ethyl acetate; for 3h; Ambient temperature;
DOI:10.1248/cpb.32.1854

Reference yield:

: 150-76-5
4-methoxy-phenol

: 69693-44-3
α-ethyl-m-nitrocinnamic acid chloride

: p-methoxyphenyl m-nitro-α-ethylcinnamate

Guidance literature:: In ethyl acetate;

Reference yield:

: 69693-44-3
α-ethyl-m-nitrocinnamic acid chloride

: 93130-88-2
phenyl α-ethyl-m-aminocinnamate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethyl acetate / 3 h / Ambient temperature

2: 1) Zn; 2) HCl / 1) acetic acid, RT; 2) Et₂O

With hydrogenchloride; triethylamine; zinc; In ethyl acetate;
DOI:10.1248/cpb.32.1854