1,4-Diphenyl-2-(phenylsulfanyl)butane-1,4-dione

Base Information

Chemical Name:1,4-Diphenyl-2-(phenylsulfanyl)butane-1,4-dione
CAS No.:69971-47-7
Molecular Formula:C22H18O2S
Molecular Weight:346.45
Hs Code.:
DSSTox Substance ID:DTXSID50536687

Synonyms:69971-47-7;1,4-Diphenyl-2-(phenylsulfanyl)butane-1,4-dione;DTXSID50536687

Suppliers and Price of 1,4-Diphenyl-2-(phenylsulfanyl)butane-1,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,4-Diphenyl-2-(phenylsulfanyl)butane-1,4-dione

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:346.10275099
Heavy Atom Count:25
Complexity:429

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)CC(C(=O)C2=CC=CC=C2)SC3=CC=CC=C3

Technology Process of 1,4-Diphenyl-2-(phenylsulfanyl)butane-1,4-dione

There total 5 articles about 1,4-Diphenyl-2-(phenylsulfanyl)butane-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 13735-81-4
1-styrenyloxytrimethylsilane

: 6099-23-6
1-(phenylsulfinyl)acetophenone

: 69971-47-7
1,4-Diphenyl-2-phenylthio-1,4-butandion

Guidance literature:: With tin(II) trifluoromethanesulfonate; 1-(Trimethylsilyl)imidazole; In dichloromethane; at -78 - 0 ℃;
DOI:10.1246/cl.1984.1531

Reference yield:

: 2461-95-2
3,4-Dibenzoyl-1,1,1-triphenyl-2-thia-butan

: 69971-47-7
1,4-Diphenyl-2-phenylthio-1,4-butandion

Guidance literature:: Multi-step reaction with 2 steps

1: (i) (SCN)2, Et₂O, dioxane, (ii) /BRN= 2608443/, ZnCl₂

2: NaOMe / dioxane; methanol

With sodium methylate; In 1,4-dioxane; methanol;
DOI:10.1021/jo01035a061

Reference yield:

: 959-28-4
1,4-diphenylbut-2-ene-1,4-dione

: 69971-47-7
1,4-Diphenyl-2-phenylthio-1,4-butandion

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / benzene / Ambient temperature

2: (i) (SCN)2, Et₂O, dioxane, (ii) /BRN= 2608443/, ZnCl₂

3: NaOMe / dioxane; methanol

With piperidine; sodium methylate; In 1,4-dioxane; methanol; benzene;
DOI:10.1021/jo01035a061