n,n'-[(2,3,5,6-Tetramethylbenzene-1,4-diyl)dimethanediyl]diacetamide

Base Information

• Chemical Name: n,n'-[(2,3,5,6-Tetramethylbenzene-1,4-diyl)dimethanediyl]diacetamide
• CAS No.: 93142-38-2
• Molecular Formula: C₁₆H₂₄N₂O₂
• Molecular Weight: 276.379
• European Community (EC) Number: 654-621-2
• NSC Number: 128522
• DSSTox Substance ID: DTXSID60299155
• Wikidata: Q82041380
• Mol file: 93142-38-2.mol

Synonyms:93142-38-2;NSC128522;n,n'-[(2,3,5,6-tetramethylbenzene-1,4-diyl)dimethanediyl]diacetamide;DTXSID60299155;AKOS024323073;NSC-128522;N,N'-(2,3,5,6-TETRAMETHYL-1,4-XYLYLENE)BISACETAMIDE

Chemical Property of n,n'-[(2,3,5,6-Tetramethylbenzene-1,4-diyl)dimethanediyl]diacetamide

Chemical Property:

• Boiling Point: 564°Cat760mmHg
• Flash Point: 212.2°C
• Density: 1.042g/cm³
• XLogP3: 1.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 276.183778013
• Heavy Atom Count: 20
• Complexity: 306

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C(=C(C(=C1CNC(=O)C)C)C)CNC(=O)C)C

Technology Process of n,n'-[(2,3,5,6-Tetramethylbenzene-1,4-diyl)dimethanediyl]diacetamide

There total 2 articles about n,n'-[(2,3,5,6-Tetramethylbenzene-1,4-diyl)dimethanediyl]diacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(4-(aminomethyl)-2,3,5,6-tetramethylphenyl)methanamine (32321-30-5) + acetic anhydride (108-24-7) → N,N'-Diacetyl-2,3,5,6-tetramethyl-1,4-di--benzol (93142-38-2)

Guidance literature:

at 80 ℃;

DOI:10.1002/chem.202003680

Reference yield:

→ N,N'-Diacetyl-2,3,5,6-tetramethyl-1,4-di--benzol (93142-38-2)

Guidance literature:

1,2,4,5-Tetramethyl-3,6-bis-hydroxymethyl-benzol, 23 Mol Acetonitril, konz.H2SO4, T= 0-30grad;

DOI:10.1021/jo01073a006

upstream raw materials:

(4-(aminomethyl)-2,3,5,6-tetramethylphenyl)methanamine

acetic anhydride