Benzene, 1-(2-nitroethenyl)-3-phenoxy-

Base Information

Chemical Name:Benzene, 1-(2-nitroethenyl)-3-phenoxy-
CAS No.:70599-84-7
Molecular Formula:C14H11NO3
Molecular Weight:241.246
Hs Code.:
DSSTox Substance ID:DTXSID40369749

Synonyms:1-(2-nitroethenyl)-3-phenoxybenzene;70599-84-7;Benzene, 1-(2-nitroethenyl)-3-phenoxy-;Oprea1_516994;DTXSID40369749

Suppliers and Price of Benzene, 1-(2-nitroethenyl)-3-phenoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzene, 1-(2-nitroethenyl)-3-phenoxy-

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:241.07389321
Heavy Atom Count:18
Complexity:292

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)OC2=CC=CC(=C2)C=C[N+](=O)[O-]

Technology Process of Benzene, 1-(2-nitroethenyl)-3-phenoxy-

There total 3 articles about Benzene, 1-(2-nitroethenyl)-3-phenoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 77124-20-0
(E)-3-(3-phenoxyphenyl)acrylic acid

: 70599-84-7
α-(m-Phenoxy)phenyl-β-nitroethene

Guidance literature:: With tert.-butylnitrite; copper(l) chloride; In acetonitrile; at 80 ℃;
DOI:10.1039/c3ob41408f

Reference yield: 70.0%

: 75-52-5
nitromethane

: 39515-51-0
3-Phenoxybenzaldehyde

: 70599-84-7
α-(m-Phenoxy)phenyl-β-nitroethene

Guidance literature:

Reference yield:

: 39515-51-0
3-Phenoxybenzaldehyde

: 70599-84-7
α-(m-Phenoxy)phenyl-β-nitroethene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 60 °C

2: sodium hydroxide / ethanol; water / 60 °C

3: copper(l) chloride; tert.-butylnitrite / acetonitrile / 80 °C

With tert.-butylnitrite; sodium hydride; copper(l) chloride; sodium hydroxide; In tetrahydrofuran; ethanol; water; acetonitrile; mineral oil;
DOI:10.1039/c3ob41408f