Technology Process of [1,1'-Biphenyl]-2-carboxylic acid,
2-([1,1'-biphenyl]-2-ylcarbonyl)-1,2-dimethoxyhydrazide
There total 10 articles about [1,1'-Biphenyl]-2-carboxylic acid,
2-([1,1'-biphenyl]-2-ylcarbonyl)-1,2-dimethoxyhydrazide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tert-butylethylene;
In
benzene;
for 2h;
Irradiation;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92.8 percent / hydroxylamine hydrochloride, sodium carbonate, water / diethyl ether
2: 87.2 percent / sodium carbonate / ethanol; H2O
3: 16 percent Spectr. / potassium t-butoxide, bromine / benzene / 2 h / Ambient temperature; further reagent
With
hydroxylamine hydrochloride; potassium tert-butylate; water; bromine; sodium carbonate;
In
diethyl ether; ethanol; water; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 0.85 g / t-butyl hypochlorite, bromine / CH2Cl2 / 5 h
2: 10 percent Spectr. / silver tetrafluoroborate
3: 16 percent Spectr. / potassium t-butoxide, bromine / benzene / 2 h / Ambient temperature; further reagent
With
silver tetrafluoroborate; tert-butylhypochlorite; potassium tert-butylate; bromine;
In
dichloromethane; benzene;
