Silacyclopent-4-en-3-ol, 1,1-diphenyl-

Base Information

• Chemical Name: Silacyclopent-4-en-3-ol, 1,1-diphenyl-
• CAS No.: 71404-32-5
• Molecular Formula: C16H16OSi
• Molecular Weight: 252.388
• DSSTox Substance ID: DTXSID50455506
• Nikkaji Number: J874.014C

Synonyms:Silacyclopent-4-en-3-ol, 1,1-diphenyl-;71404-32-5;DTXSID50455506;1,1-Diphenyl-1-sila-2-cyclopenten-4-ol

Chemical Property of Silacyclopent-4-en-3-ol, 1,1-diphenyl-

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 252.097041664
• Heavy Atom Count: 18
• Complexity: 282

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C(C=C[Si]1(C2=CC=CC=C2)C3=CC=CC=C3)O

Technology Process of Silacyclopent-4-en-3-ol, 1,1-diphenyl-

There total 2 articles about Silacyclopent-4-en-3-ol, 1,1-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

3,3-diphenyl-6-oxa-3-silabicyclo[3.1.0]hexane (51343-26-1) → 1,1-diphenylsilacyclopent-2-en-4-ol (71404-32-5)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

DOI:10.1021/ol101453e

Reference yield:

→ 1,1-diphenylsilacyclopent-2-en-4-ol (71404-32-5)

Guidance literature:

DOI:10.1007/BF00947422

Reference yield: 70.0%

1,1-diphenylsilacyclopent-2-en-4-ol (71404-32-5) → (Z)-buta-1,3-dienyldiphenylsilanol (1241514-98-6)

Guidance literature:

With p-toluenesulfonyl chloride; In pyridine; at 0 ℃; Inert atmosphere;

DOI:10.1021/ol101453e

upstream raw materials:

3,3-diphenyl-6-oxa-3-silabicyclo[3.1.0]hexane

Downstream raw materials:

(Z)-buta-1,3-dienyldiphenylsilanol

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