1-Cyclohexene-1-carboxylic acid, 2-[(diethoxyphosphinyl)oxy]-, methylester

Base Information

Chemical Name:1-Cyclohexene-1-carboxylic acid, 2-[(diethoxyphosphinyl)oxy]-, methylester
CAS No.:71712-64-6
Molecular Formula:C12H21O6P
Molecular Weight:292.269
Hs Code.:

Synonyms:1-Cyclohexene-1-carboxylic acid, 2-[(diethoxyphosphinyl)oxy]-, methylester

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Chemical Property of 1-Cyclohexene-1-carboxylic acid, 2-[(diethoxyphosphinyl)oxy]-, methylester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1-Cyclohexene-1-carboxylic acid, 2-[(diethoxyphosphinyl)oxy]-, methylester

There total 2 articles about 1-Cyclohexene-1-carboxylic acid, 2-[(diethoxyphosphinyl)oxy]-, methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 814-49-3
diethyl chlorophosphate

: 41302-34-5
2-(methoxycarbonyl)cyclohexanone

: 71712-64-6
2-(Diethoxy-phosphoryloxy)-cyclohex-1-enecarboxylic acid methyl ester

Guidance literature:: Multistep reaction; (i) NaH, Et₂O, (ii) /BRN= 471433/;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 71712-64-6
2-(Diethoxy-phosphoryloxy)-cyclohex-1-enecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride; potassium hydride / tetrahydrofuran / 1.5 h / Inert atmosphere; Reflux

1.2: Cooling with ice; Inert atmosphere

2.1: sodium hydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

With potassium hydride; sodium hydride; In tetrahydrofuran; diethyl ether;
DOI:10.15227/orgsyn.062.0014