6-Octen-3-one, 2,6-dimethyl-8-(phenylsulfonyl)-, (E)-

Base Information

Chemical Name:6-Octen-3-one, 2,6-dimethyl-8-(phenylsulfonyl)-, (E)-
CAS No.:72049-76-4
Molecular Formula:C16H22O3S
Molecular Weight:294.415
Hs Code.:

Synonyms:

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Chemical Property of 6-Octen-3-one, 2,6-dimethyl-8-(phenylsulfonyl)-, (E)-

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Technology Process of 6-Octen-3-one, 2,6-dimethyl-8-(phenylsulfonyl)-, (E)-

There total 4 articles about 6-Octen-3-one, 2,6-dimethyl-8-(phenylsulfonyl)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 74832-85-2
6,7-oxido-3,7-dimethyl-1-(benzenesulfonyl)-(2E)-octene

: 72049-76-4
2,6-Dimethyl-8-(phenylsulfonyl)-6(E)-octen-3-one

Guidance literature:: With lithium perchlorate; tetraethylammonium perchlorate; In dichloromethane; Ambient temperature; electrolysis, platinum electrodes, 0.03 F/mol;
DOI:10.1016/S0040-4039(00)88043-0

Reference yield:

: 106-25-2
Nerol

: 72049-76-4
2,6-Dimethyl-8-(phenylsulfonyl)-6(E)-octen-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 1) PBr₃ / 1. ether, 3 h, room temp.; 2. DMF,20 h , room temp.

2: 88 percent / NaBr / acetonitrile; H₂O / 2 h / 25 - 28 °C / Electrolysis, 10 mA, 2-3 V, platinum electrode

3: formic acid / formic acid / 2 h / 100 °C / under N₂

With formic acid; phosphorus tribromide; sodium bromide; In formic acid; water; acetonitrile;
DOI:10.1021/jo01289a003

Reference yield:

: 56691-80-6
geranyl phenyl sulfone

: 72049-76-4
2,6-Dimethyl-8-(phenylsulfonyl)-6(E)-octen-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / NaBr / acetonitrile; H₂O / 2 h / 25 - 28 °C / Electrolysis, 10 mA, 2-3 V, platinum electrode

2: formic acid / formic acid / 2 h / 100 °C / under N₂

With formic acid; sodium bromide; In formic acid; water; acetonitrile;
DOI:10.1021/jo01289a003