(2-AMino-thiazol-5-yl)-acetic acid Methyl ester hydrobroMide

Base Information

• Chemical Name: (2-AMino-thiazol-5-yl)-acetic acid Methyl ester hydrobroMide
• CAS No.: 723278-34-0
• Molecular Formula: C6H8N2O2S.BrH
• Molecular Weight: 253.12
• Hs Code.: 2934100090
• Mol file: 723278-34-0.mol

Synonyms:Methyl 2-(2-aminothiazol-5-yl)acetate hydrobromide;methyl (2-amino-1,3-thiazol-5-yl) acetate hydrobromide;(2-amino-thiazol-5-yl)-acetic acid methyl ester hydrobromide;C-8014;

Chemical Property of (2-AMino-thiazol-5-yl)-acetic acid Methyl ester hydrobroMide

Chemical Property:

• PSA: 94.18000
• LogP: 1.32900
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

Methyl 2-(2-amino-1,3-thiazol-5-yl)acetate hydrobromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-AMino-thiazol-5-yl)-acetic acid Methyl ester hydrobroMide

There total 1 articles about (2-AMino-thiazol-5-yl)-acetic acid Methyl ester hydrobroMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

methyl 3-bromo-4-oxobutanoate (16565-77-8) + thiourea (17356-08-0) → methyl 2-(2-aminothiazol-5-yl)acetate hydrobromide (723278-34-0)

Guidance literature:

In methanol; at 20 - 80 ℃; for 102h;

Reference yield: 100.0%

methyl 2-(2-aminothiazol-5-yl)acetate hydrobromide (723278-34-0) → 2-(2-aminothiazol-5-yl)acetic acid (52454-66-7)

Guidance literature:

methyl 2-(2-aminothiazol-5-yl)acetate hydrobromide; With sodium hydroxide; water; In methanol; at 20 ℃; for 3h;

With hydrogenchloride; In water; pH=3.5;

Reference yield: 98.0%

methyl 2-(2-aminothiazol-5-yl)acetate hydrobromide (723278-34-0) + di-tert-butyl dicarbonate (24424-99-5) → methyl (2-((tert-butoxycarbonyl)amino)-1,3-thiazol-5-yl)acetate (385785-37-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; water; at 0 - 20 ℃; for 20h;

upstream raw materials:

methyl 3-bromo-4-oxobutanoate

thiourea

Downstream raw materials:

methyl (2-((tert-butoxycarbonyl)amino)-1,3-thiazol-5-yl)acetate

2-(2-aminothiazol-5-yl)acetic acid

C₁₄H₁₁ClN₄O₃S

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