Technology Process of 3-Cyclohexene-1-carboxylic acid, 5-[bis(phenylsulfonyl)methyl]-, methyl
ester, trans-
There total 6 articles about 3-Cyclohexene-1-carboxylic acid, 5-[bis(phenylsulfonyl)methyl]-, methyl
ester, trans- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triphenylphosphine;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
for 24h;
Heating;
further solvent (DMSO);
DOI:10.1021/ja00534a029
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 82 percent / sodium methoxide / 10 h / Ambient temperature
2: 77 percent / perchloric acid / ethyl acetate; H2O / 2 h / Ambient temperature
3: 70 percent / sodium methoxide / methanol / 7.5 h / Ambient temperature
4: 40 percent / sodium methoxide / benzene / 3 h / Heating
5: pyridine / 9 h / Ambient temperature
6: 92 percent / triphenylphosphine / tetrakis(triphenylphosphine)palladium(0) / tetrahydrofuran / 24 h / Heating; further solvent (DMSO)
With
pyridine; perchloric acid; sodium methylate; triphenylphosphine;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; methanol; water; ethyl acetate; benzene;
DOI:10.1021/ja00534a029
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 40 percent / sodium methoxide / benzene / 3 h / Heating
2: pyridine / 9 h / Ambient temperature
3: 92 percent / triphenylphosphine / tetrakis(triphenylphosphine)palladium(0) / tetrahydrofuran / 24 h / Heating; further solvent (DMSO)
With
pyridine; sodium methylate; triphenylphosphine;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; benzene;
DOI:10.1021/ja00534a029
