2H-Isoxazolo[4,5-d]azepin-3(4H)-one,5,6,7,8-tetrahydro-(9CI)

Base Information

Chemical Name:2H-Isoxazolo[4,5-d]azepin-3(4H)-one,5,6,7,8-tetrahydro-(9CI)
CAS No.:53658-58-5
Molecular Formula:C₇H₁₀N₂O₂
Molecular Weight:154.169
Hs Code.:2934999090
Mol file:53658-58-5.mol

Synonyms:2H-Isoxazolo[4,5-d]azepin-3(4H)-one,5,6,7,8-tetrahydro- (9CI); 5,6,7,8-Tetrahydro-4H-isoxazolo[4,5-d]azepin-3-ol;THAZ

Suppliers and Price of 2H-Isoxazolo[4,5-d]azepin-3(4H)-one,5,6,7,8-tetrahydro-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2H-Isoxazolo[4,5-d]azepin-3(4H)-one,5,6,7,8-tetrahydro-(9CI)

Chemical Property:

Vapor Pressure:1.59E-05mmHg at 25°C
Boiling Point:354.9°Cat760mmHg
Flash Point:168.4°C
PSA：58.29000
Density:1.29g/cm³
LogP:0.39720

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2H-Isoxazolo[4,5-d]azepin-3(4H)-one,5,6,7,8-tetrahydro-(9CI)

There total 4 articles about 2H-Isoxazolo[4,5-d]azepin-3(4H)-one,5,6,7,8-tetrahydro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53601-35-7
ethyl 3-hydroxy-4,5,7,8-tetrahydro-6H-isoxazolo-[4,5-d]azepine-6-carboxylate

: 53658-58-5
THAZ

Guidance literature:: With hydrogen bromide; In acetic acid;

Reference yield:

: 53601-33-5
diethyl 1,4-dioxa-8-azaspiro[4.6]undecane-8,11-dicarboxylate

: 53658-58-5
THAZ

Guidance literature:: Multi-step reaction with 3 steps

1: NH₂OH, KOH / methanol

2: aq. HCl / methanol

3: aq. HBr / acetic acid

With hydrogenchloride; potassium hydroxide; hydrogen bromide; hydroxylamine; In methanol; acetic acid;

Reference yield:

: 53601-34-6
ethyl 11-(hydroxycarbamoyl)-1,4-dioxa-8-azaspiro[4.6]undecane-8-carboxylate

: 53658-58-5
THAZ

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / methanol

2: aq. HBr / acetic acid

With hydrogenchloride; hydrogen bromide; In methanol; acetic acid;